Table 3. Derivatives of Series 8 Synthesized with Various Aldehydes along with Obtained Results.
entry | producta | R | yieldb (%) | Rf value | melting point (°C) |
---|---|---|---|---|---|
1 | 8a | C6H5 | 67 | 0.76 | 158–15943,48 |
2 | 8b | 4-NO2-C6H4 | 74 | 0.53 | 172–173 |
3 | 8c | 4-Me-C6H4 | 69 | 0.72 | 148–150 |
4 | 8d | 4-OMe-C6H4 | 66 | 0.67 | 156–157 |
5 | 8e | 2-OH-C6H4 | 71 | 0.61 | 176–178 |
6 | 8f | 3-NO2-C6H4 | 70 | 0.57 | 167–16842 |
7 | 8g | 4-OH, 3-OCH3 C6H3 | 70 | 0.48 | 181–182 |
8 | 8h | C6H4-CH=CH | 66 | 0.65 | 164–165 |
9 | 8i | 2-pyridinyl | 42 | 0.61 | 145–148 |
10 | 8j | 2-furyl | 76 | 0.69 | 147–149 |
11 | 8k | 2-thiophenyl | 74 | 0.66 | 151–152 |
Products were characterized with standard and reliable spectral techniques.
Yield refers to the total extraction from different crops.