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. 2022 Apr 28;7(18):16055–16062. doi: 10.1021/acsomega.2c01316

Table 3. Derivatives of Series 8 Synthesized with Various Aldehydes along with Obtained Results.

entry producta R yieldb (%) Rf value melting point (°C)
1 8a C6H5 67 0.76 158–15943,48
2 8b 4-NO2-C6H4 74 0.53 172–173
3 8c 4-Me-C6H4 69 0.72 148–150
4 8d 4-OMe-C6H4 66 0.67 156–157
5 8e 2-OH-C6H4 71 0.61 176–178
6 8f 3-NO2-C6H4 70 0.57 167–16842
7 8g 4-OH, 3-OCH3 C6H3 70 0.48 181–182
8 8h C6H4-CH=CH 66 0.65 164–165
9 8i 2-pyridinyl 42 0.61 145–148
10 8j 2-furyl 76 0.69 147–149
11 8k 2-thiophenyl 74 0.66 151–152
a

Products were characterized with standard and reliable spectral techniques.

b

Yield refers to the total extraction from different crops.