Table 4. Derivatives of Series 9 Synthesized with Various Aldehydes along with Obtained Results.
entry | producta | R | yield (%) | Rf value | melting point (°C) |
---|---|---|---|---|---|
1 | 9a | C6H5 | 91 | 0.45 | 219–220 |
2 | 9b | 4-NO2-C6H4 | 94 | 0.69 | 233–235 |
3 | 9c | 4-Me-C6H4 | 85 | 0.59 | 194–196 |
4 | 9d | 4-OMe-C6H4 | 89 | 0.52 | 209–210 |
5 | 9e | 2-OH-C6H4 | 83 | 0.64 | 221–222 |
6 | 9f | 3-NO2-C6H4 | 85 | 0.60 | 229–230 |
7 | 9g | 4-OH, 3-OCH3 C6H3 | 90 | 0.61 | 247–249 |
8 | 9h | C6H4-CH=CH | 81 | 0.53 | 216–217 |
9 | 9i | 2-pyridinyl | 64 | 0.66 | 209–210 |
10 | 9j | 2-furyl | 92 | 0.72 | 189–191 |
11 | 9k | 2-thiophenyl | 90 | 0.68 | 192–193 |
Products were characterized with standard and reliable spectral techniques.