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. 2022 Apr 29;10:885487. doi: 10.3389/fchem.2022.885487

TABLE 2.

13C (150 MHz) NMR data of compounds 1–6 in pyrdine-d5.

No. 1 2 3 4 5 6
1 33.3, CH2 33.3, CH2 32.9, CH2 33.0, CH2 35.0, CH2 35.1, CH2
2 151.4, C 151.4, C 149.9, C 149.8, C 71.3, CH 71.3, CH
3 155.7, C 155.7, C 157.3, C 157.3, C 81.8, CH 81.8, CH
4 42.7, C 42.7, C 42.9, C 42.9, C 43.2, C 43.2, C
5 142.1, C 142.1, C 142.0, C 142.0, C 142.9, C 142.8, C
6 121.0, CH 121.0, CH 121.1, CH 121.1, CH 119.0, CH 119.0, CH
7 24.5, CH2 24.5, CH2 24.5, CH2 24.5, CH2 24.6, CH2 24.6, CH2
8 43.3, CH 43.4, CH 43.2, CH 43.4, CH 43.1, CH 43.2, CH
9 49.1, C 49.1, C 49.1, C 49.1, C 49.4, C 49.6, C
10 36.3, CH 36.2, CH 36.6, CH 36.5, CH 34.5, CH 34.5, CH
11 213.7, C 213.8, C 213.6, C 213.7, C 213.2, C 213.5, C
12 49.7, CH2 49.6, CH2 49.7, CH2 49.6, CH2 49.1, CH2 49.2, CH2
13 51.3, C 51.4, C 51.3, C 51.4, C 48.5, C 49.1, C
14 49.1, C 49.0, C 49.1, C 49.0, C 49.6, C 48.9, C
15 46.7, CH2 46.8, CH2 46.7, CH2 46.8, CH2 41.0, CH2 41.8, CH2
16 70.7, CH 71.0, CH 70.7, CH 71.0, CH 70.8, CH 77.0, CH
17 59.4, CH 60.2, CH 59.4, CH 60.2, CH 55.4, CH 56.3, CH
18 20.2, CH3 20.3, CH3 20.2, CH3 20.2, CH3 20.2, CH3 21.0, CH3
19 20.8, CH3 21.0, CH3 20.8, CH3 21.0, CH3 21.0, CH3 20.6, CH3
20 80.5, C 80.2, C 81.9, C 80.2, C 72.6, C 71.8, C
21 25.9, CH3 26.0, CH3 25.9, CH3 26.0, CH3 29.0, CH3 25.8, CH3
22 215.4, C 204.7, C 215.5, C 204.8, C 49.6, CH2 50.0, CH2
23 32.6, CH2 122.8, CH 32.6, CH2 122.8, CH 110.0, C 73.7, CH
24 35.7, CH2 150.2a, CH 35.8, CH2 150.2a, CH 42.2, CH2 126.2, CH
25 81.9, C 80.0, C 80.5, C 80.0, C 40.6, CH 138.5, C
26 26.3, CH3 26.5, CH3 26.3, CH3 26.5, CH3 64.8, CH2 67.6, CH2
27 26.4, CH3 26.9, CH3 26.4, CH3 26.9, CH3 71.1, CH2 14.7, CH3
28 32.0, CH3 32.1, CH3 31.6, CH3 31.7, CH3 25.8, CH3 30.0, CH3
29 30.7, CH3 30.7, CH3 30.9, CH3 30.8, CH3 22.6, CH3 22.7, CH3
30 19.3, CH3 19.3, CH3 19.3, CH3 19.3, CH3 21.7, CH3 21.6, CH3
32 144.2, CH 144.2, CH 143.3, C 143.2, C — —
33 153.8, C 153.8, C 154.6, CH 154.5, CH — —
35 40.4, CH2 40.4, CH2 40.4, CH2 40.4, CH2 — —
36 73.5, CH 73.5, CH 73.6, CH 73.6, CH — —
37 76.8, CH 76.8, CH 76.7, CH 76.7, CH — —
38 65.5, CH2 65.5, CH2 65.4, CH2 65.4, CH2 — —
39 170.5, C 170.2, C 170.5, C 170.2, C — —
40 22.6, CH3 22.1, CH3 22.6, CH3 22.1, CH3 — —