Table 2.
No. | RIdet a | RIref b | Compound c | FGMT d | WJYH | CH | BYZH | EQ | JY | LBS | HBS | THFC | ZF | MJH |
---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
1 | - | 800 | Octane | 0.1 | 0.1 | 0.7 | 0.1 | 0.6 | 2.3 | 0.6 | 0.4 | 0.9 | 0.3 | 1.3 |
2 | 802 | 801 | Hexanal | 0.2 | 0.3 | - | 0.3 | 0.4 | - | 1.0 | 1.0 | 0.9 | 0.3 | 1.2 |
3 | 852 | 854 | trans-2-Hexenal | - | - | - | - | - | 0.2 | - | 0.2 | - | - | - |
4 | 860 | 858 | cis-3-Hexen-1-ol | 1.4 | 2.1 | 2.3 | 2.9 | 3.2 | 4.2 | 1.2 | 4.0 | 1.9 | 1.7 | 1.5 |
5 | 870 | 868 | 1,4-Dimethylbenzene | 0.1 | - | - | 0.2 | 0.2 | - | - | 0.3 | tr | 0.1 | 0.1 |
6 | 873 | 871 | 1-Hexanol | 1.7 | 3.7 | 2.1 | 2.9 | 2.5 | 2.9 | 0.7 | 3.6 | 1.0 | 1.2 | 0.9 |
7 | 882 | 882 | 2,6-Dimethyl-1,5-heptadiene | 0.3 | - | - | 0.4 | - | 0.8 | 0.3 | - | - | 0.3 | - |
8 | 899 | 900 | Nonane | - | - | - | - | - | 0.2 | - | - | - | - | - |
9 | 903 | 902 | Heptanal | - | - | 0.2 | - | 0.1 | 0.5 | 0.2 | 0.2 | - | - | 0.3 |
10 | 931 | 932 | α-Pinene | 0.2 | - | - | - | - | 0.5 | 0.2 | - | - | - | - |
11 | 989 | 989 | Prenylacetone | 0.3 | - | - | 0.3 | - | 0.4 | - | - | - | - | - |
12 | 992 | 993 | 2-Pentylfuran | - | - | - | - | - | - | - | - | 0.3 | - | - |
13 | 1005 | 1004 | Octanal | - | - | - | - | - | 0.2 | - | - | - | - | - |
14 | 1038 | 1037 | cis-β-Ocimene | - | - | - | tr | - | - | - | - | - | - | - |
15 | 1049 | 1048 | trans-β-Ocimene | 0.3 | - | - | 6.7 | - | - | - | - | - | - | - |
16 | 1050 | 1046 | Benzeneacetaldehyde | - | - | - | - | - | - | - | tr | - | - | - |
17 | 1075 | 1074 | cis-Linalool oxide furan | 1.2 | 0.2 | 2.0 | 1.5 | - | 1.6 | 0.7 | 1.1 | 1.2 | - | 0.4 |
18 | 1091 | 1088 | trans-Linalool oxide furan | 0.5 | - | 1.0 | 0.7 | - | 0.7 | 0.3 | 0.6 | 0.5 | - | - |
19 | 1099 | 1100 | Undecane | - | 0.3 | 0.4 | 0.5 | 0.7 | 0.2 | - | 0.2 | - | - | 0.2 |
20 | 1107 | 1104 | Nonanal | - | - | - | - | 3.2 | 7.2 | 4.8 | 3.8 | 5.4 | 1.8 | 6.4 |
21 | 1108 | 1106 | Linalool | 1.9 | 1.6 | 3.1 | 1.8 | - | - | - | - | - | - | - |
22 | 1113 | 1111 | cis-Rose oxide | - | - | - | - | - | 1.3 | - | - | - | 0.7 | - |
23 | 1128 | 1127 | trans-Rose oxide | - | - | - | - | - | 0.4 | - | - | - | 0.3 | - |
24 | 1130 | 1127 | Benzeneethanol | - | - | - | - | - | - | - | 4.0 | 0.4 | - | - |
25 | 1164 | 1160 | cis-3-Nonen-1-ol | - | - | - | - | - | - | - | - | 0.4 | - | - |
26 | 1171 | 1170 | Hydroquinone dimethyl ether | 4.1 | 2.7 | 0.4 | - | 2.5 | - | - | - | - | 0.2 | - |
27 | 1181 | 1176 | 1-Nonanol | - | - | - | - | 0.5 | 0.9 | - | - | - | - | - |
28 | 1184 | 1180 | Myrtanal | - | - | - | - | - | - | - | 0.3 | 0.8 | - | - |
29 | 1199 | 1200 | Dodecane | - | 0.5 | - | - | 0.2 | - | - | - | - | - | - |
30 | 1202 | 1201 | α-Terpineol | 0.3 | - | 0.8 | 0.7 | - | 0.3 | 0.7 | 0.6 | 0.3 | - | - |
31 | 1208 | 1208 | Decanal | - | - | - | - | - | 0.3 | - | - | - | - | - |
32 | 1221 | 1220 | 4,7-Dimethylbenzofuran | 0.4 | 0.6 | 0.5 | 0.6 | 1.5 | 0.7 | 0.9 | 0.6 | 1.0 | 0.6 | 0.7 |
33 | 1237 | 1230 | Nerol | - | 0.9 | 2.5 | - | - | - | 3.6 | 4.2 | 2.5 | - | - |
34 | 1239 | 1231 | Citronellol | 7.9 | - | - | 21.6 | - | 23.1 | - | - | - | 25.8 | 2.2 |
35 | 1246 | 1240 | Neral | 1.2 | - | - | - | - | - | - | - | - | - | - |
36 | 1264 | 1256 | Geraniol | 13.0 | 2.2 | 2.4 | 3.0 | - | 5.6 | 1.7 | 3.9 | 4.2 | - | 0.7 |
37 | 1276 | 1270 | Geranial | 1.4 | - | - | 0.8 | - | 0.2 | - | - | - | - | - |
38 | 1283 | 1275 | 1-Decanol | - | - | - | - | 0.4 | - | - | - | - | - | - |
39 | 1299 | 1300 | Tridecane | 0.3 | 0.9 | 0.2 | 0.8 | 0.5 | 0.2 | 0.2 | 0.6 | 0.6 | 0.3 | 0.6 |
40 | 1327 | 1326 | Geranic acid methyl ester | - | - | - | - | - | 0.2 | - | - | - | - | - |
41 | 1355 | 1354 | Citronellyl acetate | - | - | - | - | - | 1.0 | - | - | - | 3.9 | 1.4 |
42 | 1386 | 1383 | Geranyl acetate | - | - | - | - | - | 0.3 | - | - | - | - | - |
43 | 1391 | 1385 | trans-3-Tetradecene | - | - | - | - | 0.2 | - | - | - | - | - | - |
44 | 1396 | 1393 | Geranic acid | 0.8 | - | - | 1.4 | - | - | 3.5 | 1.0 | - | 0.3 | - |
45 | 1399 | 1400 | Tetradecane | 1.3 | 1.1 | 0.7 | 1.6 | 0.9 | - | 2.2 | 2.0 | 0.4 | 0.8 | 1.4 |
46 | 1414 | 1407 | Eugenol methyl ether | - | - | 0.2 | - | - | - | - | - | - | - | - |
47 | 1423 | 1418 | Phloroglucinol trimethyl ether | 0.4 | 1.2 | 36.8 | - | 0.3 | 7.3 | 9.9 | 0.8 | 12.9 | 15.6 | - |
48 | 1457 | 1455 | Geranyl acetone | - | - | 0.1 | - | 0.2 | 0.4 | 0.2 | - | 0.3 | 0.2 | 0.3 |
49 | 1461 | 1462 | 2,6,10-Trimethyltridecane | 0.3 | 0.4 | 0.5 | 0.2 | 1.0 | 1.0 | 0.9 | 0.3 | 0.8 | 1.1 | 1.2 |
50 | 1476 | 1475 | 1,14-Pentadecadiene * | - | 0.2 | - | - | - | - | - | - | - | - | - |
51 | 1483 | 1481 | Germacrene D | 2.2 | 0.6 | 0.3 | 10.5 | 2.1 | - | 1.6 | 0.9 | 4.1 | - | 0.4 |
52 | 1484 | 1485 | Citronellyl isobutyrate | - | - | - | - | - | - | - | - | - | 0.4 | - |
53 | 1500 | 1500 | Pentadecane | 10.1 | 11.1 | 2.7 | 2.5 | 7.1 | 1.9 | 2.3 | 13.2 | 9.0 | 3.6 | 12.8 |
54 | 1510 | 1508 | α-Farnesene | - | - | 2.4 | 0.6 | 2.1 | 0.6 | 0.2 | - | - | 1.6 | 1.0 |
55 | 1526 | 1524 | δ-Cadinene | - | - | - | 0.4 | - | - | - | - | - | - | - |
56 | 1570 | 1570 | 3-Methylpentadecane | - | 0.8 | - | - | - | - | - | - | - | - | - |
57 | 1571 | 1570 | cis-9-Tridecen-1-ol * | 0.4 | - | - | - | 0.3 | - | - | 0.7 | 0.3 | - | 0.6 |
58 | 1572 | 1572 | Citronellyl 2-methylbutanoate | - | - | - | - | - | - | - | - | - | 0.7 | - |
59 | 1575 | 1577 | 1,15-Hexadecadiene * | - | 0.2 | - | - | 0.2 | - | - | 0.4 | - | - | 0.3 |
60 | 1577 | 1577 | Citronellyl 3-methylbutanoate | - | - | - | - | - | - | - | - | - | 0.8 | - |
61 | 1578 | 1579 | cis-3-Hexadecene | 0.2 | 0.3 | - | - | 0.2 | - | - | 0.3 | - | - | - |
62 | 1578 | 1580 | cis-3-Hexenyl benzoate | - | - | - | - | - | 0.1 | - | - | - | - | 0.5 |
63 | 1599 | 1600 | Hexadecane | 0.4 | 0.6 | 1.2 | - | 1.3 | 0.1 | 0.2 | 0.5 | 0.3 | 1.8 | 1.5 |
64 | 1654 | 1651 | τ-Muurolol | - | - | - | 0.6 | - | - | - | - | - | - | - |
65 | 1663 | 1665 | 2-Methylhexadecane | 0.6 | 1.6 | 0.7 | - | 1.0 | 0.3 | 0.7 | 0.6 | 0.4 | 0.7 | 0.9 |
66 | 1669 | 1667 | 6,9-Heptadecadiene | 9.0 | 15.5 | 0.8 | - | 3.2 | 1.2 | 1.1 | 12.4 | 6.4 | 1.4 | 6.1 |
67 | 1676 | 1676 | trans-8-Heptadecene | 3.8 | 4.9 | 0.4 | 0.3 | 1.1 | 0.6 | 0.4 | 4.0 | 2.0 | 0.7 | 1.9 |
68 | 1700 | 1700 | Heptadecane | 4.2 | 7.3 | 5.2 | 0.9 | 10.1 | 5.1 | 6.2 | 3.3 | 3.2 | 5.2 | 9.3 |
69 | 1713 | 1714 | 2-Pentadecanol | - | 0.8 | - | - | 0.2 | - | - | - | - | - | - |
70 | 1770 | 1770 | 3-Methylheptadecane | 0.1 | 0.8 | 0.2 | - | 0.7 | 0.4 | 0.4 | - | - | 0.3 | 0.6 |
71 | 1799 | 1800 | Octadecane | 0.3 | 0.3 | 1.4 | - | 0.7 | 0.3 | 0.5 | 0.3 | 1.1 | 0.7 | 0.7 |
72 | 1814 | 1812 | 2-Hexadecanol | - | 0.2 | - | - | - | - | - | - | - | - | - |
73 | 1820 | 1819 | Hexadecanal | - | - | - | - | - | 0.1 | - | - | - | - | - |
74 | 1848 | 1845 | Hexahydrofarnesyl acetone | - | 0.3 | 0.2 | - | 0.6 | 0.4 | 0.5 | - | 0.5 | 0.6 | 0.7 |
75 | 1863 | 1864 | 2-Methyloctadecane | - | 0.3 | - | - | 0.3 | 0.1 | - | - | - | - | - |
76 | 1873 | 1874 | 9-Nonadecene | 0.4 | 0.7 | 0.5 | - | 0.3 | 1.2 | 0.2 | 1.7 | 0.3 | 0.4 | 0.8 |
77 | 1879 | 1879 | 1,18-Nonadecadiene * | - | 1.4 | - | - | - | - | - | - | - | - | - |
78 | 1889 | 1892 | 1-Nonadecene | - | 1.2 | - | - | - | - | - | - | - | - | - |
79 | 1900 | 1900 | Nonadecane | 4.5 | 5.4 | 5.2 | 1.6 | 12.4 | 7.4 | 13.3 | 5.2 | 3.8 | 1.5 | 12.6 |
80 | 1915 | 1909 | 2-Heptadecanol | - | 1.2 | - | - | 0.5 | - | 0.2 | - | - | - | - |
81 | 1917 | 1920 | Heptadecanal | 0.2 | - | - | - | - | - | - | 0.2 | - | - | - |
82 | 1922 | 1919 | Farnesyl acetone | - | - | - | - | - | 0.3 | - | 0.2 | 0.3 | - | - |
83 | 1971 | 1972 | 3-Methylnonadecane | 0.3 | 0.6 | 0.2 | 0.2 | 0.7 | 0.4 | 0.5 | 0.2 | 0.2 | - | 0.5 |
84 | 1992 | 1984 | Hexadecanoic acid | - | - | - | - | 0.3 | - | - | 0.2 | 0.3 | - | - |
85 | 1999 | 2000 | Eicosane | 0.2 | 0.2 | 0.4 | 0.3 | 0.4 | 0.3 | 0.5 | 0.3 | 0.8 | 0.2 | 0.2 |
86 | 2027 | 2024 | Octadecanal | - | - | - | - | - | 0.4 | - | - | - | - | - |
87 | 2066 | 2069 | Linoleyl alcohol | - | 0.4 | - | - | - | - | - | - | - | - | - |
88 | 2067 | 2064 | 2-Methyleicosane | 0.2 | - | - | 0.2 | 0.2 | - | - | 0.2 | 0.2 | - | - |
89 | 2075 | 2080 | 1-Octadecanol | - | - | - | - | - | - | - | 0.2 | - | - | - |
90 | 2100 | 2100 | Heneicosane | 3.9 | 2.1 | 1.9 | 4.6 | 3.9 | 2.2 | 5.5 | 3.9 | 4.3 | 0.8 | 3.3 |
91 | 2174 | 2172 | 3-Methylheneicosane | 0.4 | 0.3 | 0.1 | 0.8 | 0.4 | 0.2 | 0.5 | 0.4 | 0.4 | - | 0.4 |
92 | 2199 | 2200 | Docosane | 0.9 | 0.5 | 1.0 | 1.3 | 0.7 | 0.4 | 1.3 | 0.7 | 1.5 | 0.7 | 0.5 |
93 | 2230 | 2229 | Eicosanal | - | - | - | - | - | 0.2 | - | - | - | - | - |
94 | 2262 | 2264 | 2-Methyldocosane | 0.4 | 0.3 | 0.2 | 0.8 | 0.4 | 0.1 | 0.4 | 0.2 | 0.2 | 0.2 | 0.2 |
95 | 2272 | 2273 | 1-Eicosanol | - | - | 0.1 | 0.2 | - | 0.1 | - | 0.2 | - | - | - |
96 | 2300 | 2300 | Tricosane | 9.4 | 9.1 | 8.6 | 13.1 | 12.3 | 4.8 | 14.3 | 7.5 | 10.8 | 8.6 | 11.7 |
97 | 2370 | 2372 | 3-Methyltricosane | 1.1 | 1.6 | 0.9 | 2.0 | 1.8 | 0.4 | 1.9 | 0.8 | 0.8 | 0.9 | 1.4 |
98 | 2399 | 2400 | Tetracosane | 0.8 | 0.8 | 1.2 | 1.0 | 1.2 | 0.5 | 1.4 | 0.6 | 1.3 | 1.3 | 0.9 |
99 | 2459 | 2462 | 2-Methyltetracosane | 0.2 | 0.4 | 0.2 | 0.4 | 0.4 | 0.1 | 0.3 | 0.1 | 0.3 | 0.3 | 0.2 |
100 | 2500 | 2500 | Pentacosane | 3.5 | 4.1 | 4.6 | 4.8 | 7.9 | 2.6 | 7.3 | 3.3 | 5.7 | 6.1 | 5.7 |
101 | 2570 | 2572 | 3-Methylpentacosane | 0.6 | 1.6 | 0.8 | 0.9 | 2.2 | 0.4 | 1.4 | 0.5 | 0.8 | 1.3 | 1.1 |
102 | 2599 | 2600 | Hexacosane | 0.2 | 0.2 | 0.2 | 0.2 | 0.4 | 0.1 | 0.4 | 0.2 | 0.4 | 0.4 | - |
103 | 2659 | 2663 | 2-Methylhexacosane | - | 0.2 | - | - | - | - | - | - | 0.3 | - | - |
104 | 2699 | 2700 | Heptacosane | 1.1 | 1.4 | 0.8 | 1.3 | 2.0 | 0.5 | 1.9 | 1.2 | 2.0 | 1.8 | 1.4 |
105 | 2770 | 2772 | 3-Methylheptacosane | 0.4 | 0.9 | 0.2 | 0.4 | 0.7 | - | 0.5 | 0.4 | 0.8 | 0.5 | 0.4 |
Sum | 99.6 | 99.2 | 99.5 | 98.9 | 99.4 | 98.9 | 99.7 | 98.7 | 99.5 | 99.0 | 99.4 |
a RIdet, retention index determined relative to C7–C30 saturated alkanes run under identical chromatographic conditions; b RIref, reference retention index retrieved from online databases of NIST Chemistry WebBook [18] (https://webbook.nist.gov/chemistry/, accessed on 20 March 2021) and ChemSpider [19] (https://www.chemspider.com/, accessed on 21 March 2021). Certain RIref values were retrieved from our previous studies [8,9]; c Compounds identified by mass spectra and retention indices; d Code for cultivar name, see Table 1. Percentages of individual components are presented as mean value of triplicate samples (RSD basically below 10% for major components); tr, trace, percentages lower than 0.05%; -, not detected; * Compounds tentatively identified.