Table 2.
Position | 13C-NMR | 1H-NMR | HMBC |
---|---|---|---|
δc (Multiplet) | δH (Multiplet, J in Hz) | H→C | |
1 | 30.7 | 1.85 (m), 1.39 (m) | C-2, C-3, C-20 |
2 | 19.8 | 1.61 (m), 2.44 (m) | C-4, C-10 |
3 | 36.7 | 1.74 (m), 1.51 (m) | C-1, C-4, C-18, C-19 |
4 | 46.3 | --- | --- |
5 | 38.1 | 2.41 (m) | C-4, C-9, C-10, C-18, C-19, C-20 |
6 | 29.7 | 1.52 (m) | C-4, C-10 |
7 | 24.2 | 2.50 (m) | C-5, C-8, C-9, C-14 |
8 | 144.1 | --- | --- |
9 | 80.7 | --- | --- |
10 | 39.0 | --- | --- |
11 | 21.7 | 2.05 (m), 1.41 (m) | C-8, C-9, C-10, C-12 |
12 | 25.0 | 1.92 (m), 1.42 (m) | C-9, C-11, C-15 |
13 | 79.1 | --- | --- |
14 | 127.0 | 6.07 (s) | C-7, C-9, C-13, C-15 |
15 | 32.1 | 1.88 (septet, J = 6.8) | C-12, C-14, C-16, C-17 |
16 | 17.4 | 0.95 (d, J = 6.8) | C-13, C-15, C-17 |
17 | 17.1 | 0.94 (d, J = 6.8) | C-13, C-15, C-16 |
18 | 184.0(s) | --- | --- |
19 | 17.5(q) | 1.26 (s) | C-3, C-4, C-5, C-19 |
20 | 19.1(q) | 1.06 (s) | C-1, C-5, C-9, C-10 |