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. 2022 Apr 23;27(9):2731. doi: 10.3390/molecules27092731

Table 2.

13C-NMR (125 MHz, Chloroform-d), 1H-NMR (500 MHz, Chloroform-d), and HMBC data for compound 3.

Position 13C-NMR 1H-NMR HMBC
δc (Multiplet) δH (Multiplet, J in Hz) H→C
1 30.7 1.85 (m), 1.39 (m) C-2, C-3, C-20
2 19.8 1.61 (m), 2.44 (m) C-4, C-10
3 36.7 1.74 (m), 1.51 (m) C-1, C-4, C-18, C-19
4 46.3 --- ---
5 38.1 2.41 (m) C-4, C-9, C-10, C-18, C-19, C-20
6 29.7 1.52 (m) C-4, C-10
7 24.2 2.50 (m) C-5, C-8, C-9, C-14
8 144.1 --- ---
9 80.7 --- ---
10 39.0 --- ---
11 21.7 2.05 (m), 1.41 (m) C-8, C-9, C-10, C-12
12 25.0 1.92 (m), 1.42 (m) C-9, C-11, C-15
13 79.1 --- ---
14 127.0 6.07 (s) C-7, C-9, C-13, C-15
15 32.1 1.88 (septet, J = 6.8) C-12, C-14, C-16, C-17
16 17.4 0.95 (d, J = 6.8) C-13, C-15, C-17
17 17.1 0.94 (d, J = 6.8) C-13, C-15, C-16
18 184.0(s) --- ---
19 17.5(q) 1.26 (s) C-3, C-4, C-5, C-19
20 19.1(q) 1.06 (s) C-1, C-5, C-9, C-10