Table 3.
Stability data for thallium.
| Storage condition | RSD, %a | Mean Percentage (%) of Day 0 |
|---|---|---|
| Extract stabilityb | ||
| Ambient extracts (5 days) | ≤ 2.6 | 98.0 – 101 |
| Refrigerated extracts (15 days, 4°C) | ≤ 0.7 | 97.2 – 101 |
| Primary Matrix stability b | ||
| Frozen samples (5 days, −20 °C) | ≤ 0.9 | 96.4 – 101 |
| Freeze–thaw (3 cycles over 3 days) | ≤ 1.6 | 98.4–100 |
| Secondary Matrix Stability c | ||
| (Up to 521 days, −80 °C) | ||
| HSDd Rat Maternal Plasma (PND4) | ≤ 2.8 | 101 – 106 |
| HSD Rat Pup Plasma (PND4) | ≤ 2.3 | 103 – 107 |
| HSD Female Rat Urine | ≤ 2.4 | 106 – 112 |
| HSD Rat Fetus | ≤ 1.9 | 93.4 – 110 |
| HSD Rat Brain | ≤ 7.3 | 99.2 – 107 |
| B6C3F1 Female Mouse Plasma | ≤ 6.6 | 99.1–109 |
RSD = percent relative standard deviation
Percent of Day 0 were determined for triplicate fortified QC samples at three levels, 2.00, 50.0, and 400 ng Tl/mL plasma.
Percent of Day 0 were determined for triplicate fortified QC samples at two levels, 2.00 and 250 ng Tl/mL matrix or ng Tl/g tissue for brain and fetus.
HSD = Harlan Sprague Dawley.