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. Author manuscript; available in PMC: 2023 Jan 1.
Published in final edited form as: Anal Lett. 2021 Dec 8;55(8):1269–1280. doi: 10.1080/00032719.2021.1993876

Table 3.

Stability data for thallium.

Storage condition RSD, %a Mean Percentage (%) of Day 0
Extract stabilityb
Ambient extracts (5 days) ≤ 2.6 98.0 – 101
Refrigerated extracts (15 days, 4°C) ≤ 0.7 97.2 – 101
Primary Matrix stability b
Frozen samples (5 days, −20 °C) ≤ 0.9 96.4 – 101
Freeze–thaw (3 cycles over 3 days) ≤ 1.6 98.4–100
Secondary Matrix Stability c
(Up to 521 days, −80 °C)
HSDd Rat Maternal Plasma (PND4) ≤ 2.8 101 – 106
HSD Rat Pup Plasma (PND4) ≤ 2.3 103 – 107
HSD Female Rat Urine ≤ 2.4 106 – 112
HSD Rat Fetus ≤ 1.9 93.4 – 110
HSD Rat Brain ≤ 7.3 99.2 – 107
B6C3F1 Female Mouse Plasma ≤ 6.6 99.1–109
a

RSD = percent relative standard deviation

b

Percent of Day 0 were determined for triplicate fortified QC samples at three levels, 2.00, 50.0, and 400 ng Tl/mL plasma.

c

Percent of Day 0 were determined for triplicate fortified QC samples at two levels, 2.00 and 250 ng Tl/mL matrix or ng Tl/g tissue for brain and fetus.

d

HSD = Harlan Sprague Dawley.