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. 2022 Apr 19;23(9):4488. doi: 10.3390/ijms23094488

Table 1.

¹H and ¹³C chemical shifts of the oligosaccharide FI and FII.

Fraction	Residue		Chemical Shift (ppm)
Fraction	Residue		1	2	3	4	5	6
FI-a	F: L-Fuc_2S-α1-	H	5.305 (J_1,2 = 4.05)	4.463	4.039	3.915	4.199	1.247
	F: L-Fuc_2S-α1-	C	100.37	77.96	69.98	74.59	70.03	17.87
	rF: -3-L-Fuc-ol	H	3.742 (J_1,1′ = 11.46)	4.055	3.769	3.707	4.189	1.227
		H	3.713 (J_1,2 = 4.96)
		C	65.51	74.35	80.88	76.80	68.53	21.37
FI-b	F′: L-Fuc_4S-α1-	H	5.124 (J_1,2 = 4.20)	3.870	4.006	4.638	4.279	1.290
	F′: L-Fuc_4S-α1-	C	101.48	70.89	71.15	83.11	69.40	18.50
	rF′: -3-L-Fuc-ol	H	3.742 (J_1,1′ = 11.46)	4.043	3.776	3.707	4.155	1.229
		H	3.713 (J_1,2 = 4.96)
		C	65.60	74.26	80.32	76.24	68.79	21.25
FII	I: L-Fuc_2S4S-α1-	H	5.332 (J_1,1 = 3.90)	4.472	4.160	4.706	4.333	1.304
	I: L-Fuc_2S4S-α1-	C	100.24	77.76	69.09	83.24	69.40	18.41
	rF: -3-L-Fuc-ol	H	3.739 (J_1,1′ = 11.40)	4.053	3.784	3.713	4.184	1.227
		H	3.710 (J_1,2 = 5.04)
		C	65.48	74.29	81.06	76.81	68.57	21.37