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. 2022 Apr 19;23(9):4488. doi: 10.3390/ijms23094488

Table 3.

¹H and ¹³C chemical shifts of the oligosaccharide FV and FVI.

Fraction	Residue		Chemical Shift (ppm)
Fraction	Residue		1	2	3	4	5	6
FV	A: L-Fuc_2S4S-α1-	H	5.306 (J_1,2 = 3.84)	4.378	4.129	4.596	4.353	1.188
	A: L-Fuc_2S4S-α1-	C	96.32	77.87	69.31	83.57	68.95	18.50
	B: -3-L-Fuc-α1-	H	4.968 (J_1,2 = 4.00)	3.832	3.892	3.968	4.336	1.147
	B: -3-L-Fuc-α1-	C	98.99	69.36	78.07	70.99	69.54	18.12
	C: -3-L-Fuc_2S -α1-	H	5.223 (J_1,2 = 3.92)	4.466	3.997	4.014	4.105	1.166
	C: -3-L-Fuc_2S -α1-	C	100.58	75.87	75.30	71.86	69.89	18.25
	D: -3-L-Fuc-ol	H	3.660 (J_{1, 1′} = 11.60) 3.636 (J_1,2 = 4.88)	3.954	3.699	3.620	4.115	1.133
	D: -3-L-Fuc-ol	C	65.61	74.53	81.25	76.86	68.71	21.49
FVI	A: L-Fuc_2S4S-α1-	H	5.245 (J_1,2 = 3.90)	4.335	4.083	4.578	4.444	1.174
	A: L-Fuc_2S4S-α1-	C	97.21	77.65	69.16	83.58	69.01	18.47
	B: -3-L-Fuc_2S-α1-	H	5.206 (J_1,2 = 3.96)	4.427	3.999	3.980	4.344	1.133
	B: -3-L-Fuc_2S-α1-	C	97.92	75.74	76.26	71.68	69.37	18.02
	C: -3-L-Fuc_2S-α1-	H	5.208 (J_1,2 = 3.92)	4.464	3.996	3.953	4.068	1.143
	C: -3-L-Fuc_2S-α1-	C	100.34	75.81	76.58	71.94	69.83	17.96
	D: -3-L-Fuc-ol	H	3.633 (J_1,1′ = 11.52) 3.603 (J_1,2 = 7.44)	3.923	3.669	3.602	4.079	1.105
	D: -3-L-Fuc-ol	C	65.44	74.43	80.92	76.77	68.63	21.34