Table 3.

HSQC spectral assignments of APEP-A-b.

Linkage type	Chemical shift (ppm)
	H-1C-1	H-2C-2	H-3C-3	H-4C-4	H-5C-5	H-6a; 6bC-6
(A) 6→)-β-D-Glcp-(1→	4.48	3.27	3.45	3.43	3.58	4.18; 3.80
	101.92	72.02	74.56	68.42	73.83	67.79
(B) 3,6→)-β-D-Glcp-(1→	4.47	3.46	3.69	3.35	3.83	3.86; 3.64
	101.95	71.82	83.36	68.53	74.17	65.59
(C) 3→)-β-D-Glcp-(1→	4.69	3.59	3.69	3.41	3.79	3.87; 3.68
	101.78	71.83	83.36	68.43	74.06	59.69
(D) β-D-Glcp-(1→	4.69	3.38	3.27	3.58	3.83	3.86; 3.68
	101.78	72.00	74.47	68.49	74.17	59.67