Skip to main content
. 2022 Apr 14;13(5):833–840. doi: 10.1021/acsmedchemlett.2c00075

Table 2. Thermal Stabilities of Diene-Acrylamide Adducts in Dowtherm Aa.

graphic file with name ml2c00075_0007.jpg

a

Amide adducts, thiophenol (3 equiv), tributylamine (3.3 equiv), and dibenzylether (1 equiv, internal standard) were dissolved in the indicated deuterated solvent and placed in a preheated NMR spectrometer. 1H spectra were collected at regular time intervals, and half-lives were calculated based upon the first order loss of starting material.