Table 1. Synthesis Condition of Copolymers and Their Composition, Molecular Weight, Polydispersity, and Thermal Properties.

run	copolymer	molar ratio DDA/TMSPA in feed	molar ratio DDA/TMSPA in product	Mn/104	Mw/Mn	Tg/°C	TM/°C	T5d/°C
1	p(DDA/TMSPA1)a	95:5	99:1	2.57	2.08	73.7	–35.2	335
2	p(DDA/TMSPA2)b	95:5	98:2	2.53	1.88	73.6	–37.2	304
3	p(DDA/TMSPA13)a,c	74:26	87:13	2.35	2.10	50.4	–35.6	349
4	p(DDA/TMSPA32)d	50:50	68:32	2.14	1.92	e	–29.8	330

^aPolymerized at 60 °C for 12 h.

^bPolymerized at 65 °C for 12 h.

^cAnother p(DDA/TMSPA13) copolymer was synthesized (Table S1).

^dPolymerized at 60 °C for 24 h.

^eUnclear.