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. 2022 May 12;15:882443. doi: 10.3389/fnmol.2022.882443

TABLE 3.

M3G pharmacological targets and effects.

References Specie/Model Experiment type M3G effects
Pasternak et al., 1987 Bovine brain membranes In vitro M3G has a low affinity for MOR
Christensen and Jorgensen, 1987 Bovine brain membranes In vitro
Chen et al., 1991 Rat brain membranes In vitro
Bartlett and Smith, 1995 Sheep brain membranes In vitro
Roeckel et al., 2017 Mouse brain membranes In vitro

Labella et al., 1979 SD male rats In vivo M3G-induced hyperalgesia/allodynia is enhanced by naloxone/naltrexone treatment
Woolf, 1981 SD rats In vivo
Yaksh et al., 1986 Rats In vivo
Yaksh and Harty, 1988 Rats In vivo
Halliday et al., 1999 SD male rats In vivo

Roeckel et al., 2017 MOR–/– mice In vivo MOR is required for M3G-induced hyperalgesia following i.p. injection

Lewis et al., 2010 SD male rats In vivo, in vitro and in silico TLR4 is required for M3G-induced hyperalgesia. M3G activates TLR4 signaling. M3G induces the release of proinflammatory cytokines.
Due et al., 2012 TLR4–/– male mice and SD female rats In vivo and in vitro
Grace et al., 2014 SD and lewis male rats In vivo, in vitro and in silico
Xie et al., 2017 HEK cells In vitro
Allette et al., 2017 SD rats In vivo and in vitro
Doyle and Murphy, 2018 SD male and female rats In vivo
Iqbal et al., 2020 PC12 cells In vitro
Wang et al., 2021 C57BL/6 mice and human lung cancer cell lines In vivo and in vitro

Sullivan et al., 1989 SD male rats In vivo electrophysiologi-cal recording M3G does not affect basal or morphine-induced inhibition of C-fiber-evoked responses of convergent dorsal horn neurons, neither on membrane currents or action potential firing in locus coeruleus neurons
Hewett et al., 1993 SD male rats In vivo electrophysiologi-cal recording
Osborne et al., 2000 SD male rats In situ electrophysiologi-cal recording

Bartlett et al., 1994a SD male rats In vivo M3G-induced behavioral excitation involves the indirect activation of NMDA receptors.
Hemstapat et al., 2003 Primary cultures of embryonic rat hippocampal neurones In vitro

Bartlett et al., 1994b SD male rats In vitro M3G does not interact with opioid, GABAA, AMPA, NMDA, kaïnate or glycinergic receptors, nor alters GABA or glutamate release from synaptosomes.
Bartlett and Smith, 1996 SD male rats In vitro

Moran and Smith, 2002 SD rats In vitro M3G reduces the amplitude of GABAerbic and glycinergic inhibitory post-synaptic currents in the rat substantia gelatinosa through a presynaptic mechanism

Komatsu et al., 2009 ddY male mice In vivo i.t. M3G-induced behavioral excitation involves the ERK-NO-cGMP-PKG pathway and is blocked by coadministration of naltriben, a selective δ2-opioid receptor antagonist
Komatsu et al., 2016 ddY male mice In vivo

Due et al., 2014 SD male and female rats In vitro M3G-induced increase of sensory neurons excitability is blocked by carbamazepine, an inhibitor of several voltage-dependent sodium channels

Arout et al., 2014 CD-1 male mice In vivo i.p. injection of M3G induces c-Fos activation in the PAG

Juni et al., 2006 CD-1 male mice In vivo M3G induces hyperalgesia following chronic treatment with high doses but not low doses of morphine

Blomqvist et al., 2020 SD male rats In vivo Chronic i.t. injections of M3G causes antinociceptive cross-tolerance to morphine and increases substance P expression in the dorsal horn of the spinal cord

Igawa et al., 1993 SD female rats In vivo i.t. M3G injection has excitatory effects on micturition

Thomas et al., 1995 Female B6C3F1 mouse cells In vitro M3G modulates B cell proliferation

Hashiguchi et al., 1995 SD male rats In vivo M3G enhance the hyperglycemic effects of M6G

AMPA, α-amino-3-hydroxy-5-methylisoxazole-4-propionate; CNS, central nervous system; ddY, Deutschland, Denken, and Yoken mice; DOR, δ-opioid receptor; DRG, dorsal root ganglion; ERK, extracellular signal-regulated kinase; GABA, γ–aminobutyric acid; GABAA, GABA receptor A; HEK, human embryonic kidney cells; KO, knock-out; KOR, κ-opioid receptor; LC, locus coeruleus; LPS, lipopolysaccharide; M3G, morphine-3-glucuronide; M6G, morphine-6-glucuronide; MD-2, myeloid differentiation factor 2; MOR, μ-opioid receptor; NF-κB, nuclear factor kappa-light-chain-enhancer of activated B cells; NMDA, N-methyl-D-aspartate; NO-cGMP-PKG, nitric oxide–cyclic guanosine monophosphate–protein kinase G signaling pathway; OIH, opioid-induced hyperalgesia; PAG, periaqueductal gray; PD-L1, programmed death-ligand 1; SD, Sprague-Dawley; TLR4, Toll-like receptor 4; vl-PAG, ventrolateral periaqueductal gray.