Table 2.
1H NMR (500 MHz) and 13C (125 MHz) NMR data for 12-hydroxyagelasidine C (3) in CDCl3.
| Position | 3 | |
|---|---|---|
| δH, Mult (J in Hz) | δC, Type | |
| 1 | 1.44, m | 27.2, CH2 |
| 2 | 1.95, m | 25.7, CH2 |
| 3 | 5.40, brs | 124.4, CH |
| 4 | 139.7, C | |
| 5 | 40.5, C | |
| 6 | 1.71, m | 33.3, CH |
| 7 | 1.43, m | 35.3, CH2 |
| 8 | 1.95, m; 1.48, m | 34.6, CH2 |
| 9 | 140.1, C | |
| 10 | 5.06, t, (6.5) | 118.6, CH |
| 11 | 2.27, t, (6.5) | 34.0, CH2 |
| 12 | 4.09, t, (6.5) | 76.3, CH |
| 13 | 149.2, C | |
| 14 | 5.52, t, (8.0) | 110.0, CH |
| 15 | 3.84, dd, (14.5, 8.0); 3.80, dd, (14.5, 8.0) | 53.8, CH2 |
| 16 | 1.71, brs | 13.1, CH3 |
| 17 | 1.61, brs | 16.6, CH3 |
| 18 | 1.60, brs | 19.3, CH3 |
| 19 | 0.84, s | 16.0, CH3 |
| 20 | 0.85, d, (6.7) | 21.2, CH3 |
| 1′ | 3.28, brs | 50.3, CH2 |
| 2′ | 3.70, brs | 34.5, CH2 |
| 3′ | 157.5, C | |