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. 2022 Apr 28;20(5):298. doi: 10.3390/md20050298

Table 2.

1H NMR (500 MHz) and 13C (125 MHz) NMR data for 12-hydroxyagelasidine C (3) in CDCl3.

Position 3
δH, Mult (J in Hz) δC, Type
1 1.44, m 27.2, CH2
2 1.95, m 25.7, CH2
3 5.40, brs 124.4, CH
4 139.7, C
5 40.5, C
6 1.71, m 33.3, CH
7 1.43, m 35.3, CH2
8 1.95, m; 1.48, m 34.6, CH2
9 140.1, C
10 5.06, t, (6.5) 118.6, CH
11 2.27, t, (6.5) 34.0, CH2
12 4.09, t, (6.5) 76.3, CH
13 149.2, C
14 5.52, t, (8.0) 110.0, CH
15 3.84, dd, (14.5, 8.0); 3.80, dd, (14.5, 8.0) 53.8, CH2
16 1.71, brs 13.1, CH3
17 1.61, brs 16.6, CH3
18 1.60, brs 19.3, CH3
19 0.84, s 16.0, CH3
20 0.85, d, (6.7) 21.2, CH3
1′ 3.28, brs 50.3, CH2
2′ 3.70, brs 34.5, CH2
3′ 157.5, C