Table 2.
Position | 3 | |
---|---|---|
δH, Mult (J in Hz) | δC, Type | |
1 | 1.44, m | 27.2, CH2 |
2 | 1.95, m | 25.7, CH2 |
3 | 5.40, brs | 124.4, CH |
4 | 139.7, C | |
5 | 40.5, C | |
6 | 1.71, m | 33.3, CH |
7 | 1.43, m | 35.3, CH2 |
8 | 1.95, m; 1.48, m | 34.6, CH2 |
9 | 140.1, C | |
10 | 5.06, t, (6.5) | 118.6, CH |
11 | 2.27, t, (6.5) | 34.0, CH2 |
12 | 4.09, t, (6.5) | 76.3, CH |
13 | 149.2, C | |
14 | 5.52, t, (8.0) | 110.0, CH |
15 | 3.84, dd, (14.5, 8.0); 3.80, dd, (14.5, 8.0) | 53.8, CH2 |
16 | 1.71, brs | 13.1, CH3 |
17 | 1.61, brs | 16.6, CH3 |
18 | 1.60, brs | 19.3, CH3 |
19 | 0.84, s | 16.0, CH3 |
20 | 0.85, d, (6.7) | 21.2, CH3 |
1′ | 3.28, brs | 50.3, CH2 |
2′ | 3.70, brs | 34.5, CH2 |
3′ | 157.5, C |