Table 2.
Chemical Shift, δ (ppm) | |||||||
---|---|---|---|---|---|---|---|
Glycosyl Linkage | Residue | H1 | H2 | H3 | H4 | H5 | H6 |
C1 | C2 | C3 | C4 | C5 | C6 | ||
1-α-D-Glcp | A | 5.38 | 3.60 | 3.70 | 3.95 | 3.97 | 3.60 |
102.72 | 71.94 | 74.03 | 70.61 | 71.68 | 62.30 | ||
1,2-α-D-Manp | B | 4.97 | 3.89 | 3.92 | 3.79 | 3.64 | 3.75 |
101.52 | 76.30 | 68.95 | 65.20 | 71.77 | 60.04 | ||
1,2-α-D-Glcp | C | 5.26 | 3.60 | 3.72 | 3.29 | 3.62 | 3.92 |
102.88 | 77.20 | 71.33 | 73.94 | 63.84 | 62.32 | ||
1,4-α-D-Glcp | D | 5.41 | 3.62 | 3.73 | 3.68 | 3.93 | 3.69 |
101.69 | 71.96 | 72.22 | 79.68 | 71.08 | 60.86 | ||
1,6-β-D-Glcp | E | 4.97 | 3.56 | 4.61 | 3.51 | 3.94 | 3.64 |
98.72 | 70.70 | 73.40 | 70.40 | 71.33 | 71.40 | ||
1,4,6-α-D-Glcp | F | 4.99 | 3.57 | 3.65 | 3.68 | 3.85 | 3.71 |
101.01 | 75.73 | 74.02 | 76.01 | 74.60 | 68.47 |