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. 2022 May 3;14(5):323. doi: 10.3390/toxins14050323

Table 8.

Bibliographic information (i.e., source) published in the last three years regarding the use of NIR for predicting mycotoxin contaminations in different matrices.

Feed Matrix Target Mycotoxin Wavelength Statistical Model * Results Obtained Practical Application Source
Ground corn samples Fumonisin B1 and B2 900–1700 nm PLS, SVM, and LPLS-S R2 prediction = 0.71–0.91
RMSEP = 12.08–22.58 mg/kg
Pocket-sized NIR spectrometers controlled by a smartphone [65]
PCA, PLS-DA, and SVM-DA Prediction accuracy = 86.3–88.2%
Error in prediction = 11.8–13.7%
Rice (Oryza sativa L.) Aflatoxin B1 400–2498 nm MSA + PLS Low-aflatoxin-level (≤35 μg/kg):
R2 calibration = 0.72–0.99
RMSEC = 0.11–5.02 μg/kg
High-aflatoxin-level (>35 μg/kg):
R2 calibration = 0.72–0.99
RMSEC = 0.56–13.74 μg/kg
Monitoring aflatoxin B1 contamination in milled rice during postharvest storage [66]
Almonds Aflatoxin B1 900–1700 nm PLS R2 = 0.786–0.958
RMSEP = 0.089–0.197 μg/g
Commercial application [67]
Distiller’s dried grains Fumonisin B1 and B2 400–2500 nm PLS FB1 R2 = 0.80
FB2 R2 = 0.79
Potential to support decision making regarding the use of feed ingredients and, consequently, to protect animal health [68]
Barley (Hordeum vulgare) Deoxynivalenol (cut off limit cut off 1250 µg/kg) 10,000 cm−1–4000 cm−1 PLS-DA Sensitivity in cross-validation = 90.9%
Specificity in cross-validation = 89.9%
Green technique to monitor DON contamination [69]
Corn products Fusarium verticillioides and F. graminearum 1000–2500 nm PLS-DA Accuracy = 99.7% Monitoring the safety of feed and food supply [70]
Wheat flour Deoxynivalenol PLS-DA and PC-LDA Contamination level ≤ 450 μg kg−1
Accuracy (PLS-DA) = 85–87.5%
Error (PLS-DA) = 10–15% error;
Accuracy (PC-LDA) = 85%
Error (PC-LDA) = 10–15% error
Screening method to evaluate DON contamination to support decision making in industries [71]

* PLS = Partial least squares; SVM = Support vector machine; LPLS-S = local PLS based on global PLS score; PCA = principal component analysis; PLS-DA = partial least squares discriminant analysis; SVM-DA = support vector machine discriminant analysis; MSA = modified simulated annealing; PC-LDA = Principal Component Analysis-Linear Discriminant Analysis.