Table 1.
Material | Quantity (mL) | Provider | Purity |
---|---|---|---|
Sulfuric acid | 4 | Sigma-Aldrich | 10 % (V/V) |
DI water | 20 | Loba Chemicals | 99.995 % |
Ethanol | 50 | Loba Chemicals | 99.5 % |
TTIP | 5 | Sigma-Aldrich | 99.99% |
Molybdenum chloride | 5 | Sigma-Aldrich | 99.9 % |
Isopropanol | 25 | Loba Chemicals | 99.5 % |
Note: When doping different transition metals onto TiO2, it is necessary to calculate the appropriate concentration and amount of the precursor based on the targeted doping percentage. In the case of the synthesis of pure TiO2, the amount of the doping metal solution was replaced with DI water to maintain the ratio of hydrolysis agents to the catalyst precursor.