Table 1. Comparison between Intended (Nominal) [Mo₃S₁₃]^2– Loadings and Those Found in the As-Prepared [Mo₃S₁₃]/TiO₂ Samples by Means of TXRF Quantification of Mo Content.

nominal [Mo3S13]2– loadings (wt %)	real [Mo3S13]2– loadings (wt %)
0.1	0.14 ± 0.01
0.5	0.50 ± 0.05
2.0	1.78 ± 0.18
3.0	2.63 ± 0.26
5.0	4.22 ± 0.42
7.0	5.22 ± 0.52
10.0	8.30 ± 0.83
20.0	9.10 ± 0.91