Skip to main content
. 2022 May 19;12(11):6596–6605. doi: 10.1021/acscatal.2c00710

Table 2. Solvent Effect in the Acetoxylation of 1a.

graphic file with name cs2c00710_0012.jpg

entry solvent yield (%)a
1 AcOH 86
2 toluene 7
3 4-CF3-C6H5 21
4 DCE 21
5 DMF  
6 iPrOH  
7 1,4-dioxane  
8 HFIP 46
9b HFIP 61
a

Determined by 1H NMR spectroscopy in the reaction crude.

b

Reaction run for 18 h.