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. 2022 Jun 10;12:9614. doi: 10.1038/s41598-022-13552-z

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© The Author(s) 2022

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/.

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Dynamic of (a) Fe(2+) and (b) Fe(3+) detected at t0, t1 and t2 in the fecal supernatant of all 11 patients. The statistical analysis was performed using the non-parametric one-way ANOVA (Kruskal–Wallis) as non-pairing due to the missing measurements of patients A16, A17 and A19 at t2. The significance threshold was set at p = 0.05. For Fe(2+) ** = 0.0028 and *** = 0.0003; while for Fe(3+) * = 0.0424 and ** = 0.0085.