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. 2022 Jun 1;7(23):19166–19175. doi: 10.1021/acsomega.2c00079

Table 4. Thermal Gradient between Heating and Stabilized Temperature.

heating temperature (°C) 40 80 120
average stabilized axial temperature (°C) 38.6 75.8 113.0
absolute error (°C) –1.4 –4.2 –7
water flow rate (mL/min) length to reach 99% of the stabilized temperature (m) – corresponding reactor volume (mL)
2 1.60–1.26 1.9–1.50 2.0–1.57
5 13.6–10.69 16.3–12.80 17.2–13.5
10 22.0–17.28 23.0–18.06 23.6–18.54