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. 2022 Jun 21;12(28):18215–18223. doi: 10.1039/d2ra02693g

Orthogonal experimental results of preparation of low molecular polyamide.

Factors Reaction time/h Reaction temperature/°C Ratio of raw materials Amine value/mg KOH g−1 Viscosity/Pa s
Experiment 1 1.5 160 2 427 62.125
Experiment 2 1.5 180 2.5 592 6.265
Experiment 3 1.5 200 3 680 3.428
Experiment 4 2 160 2.5 676 16.700
Experiment 5 2 180 3 740 4.178
Experiment 6 2 200 2 595 50.371
Experiment 7 2.5 160 3 744 4.670
Experiment 8 2.5 180 2 493 73.120
Experiment 9 2.5 200 2.5 628 9.362