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. 2022 Jun 9;15:100315. doi: 10.1016/j.mtbio.2022.100315

Table 1.

Summary of animal in vivo studies which evaluated immunological parameters after Mg-based biomaterials implantation.

Article author Year Implant material/shape/size Animal species and number Implantation site Histology specimen Study length Methods used for testing immunological reaction Parameters evaluated
Castellani et al. [50] 2010 Mg–Y-Nd-HRE (Titanium group as control)
Shape: cylindrical
Diameter: 1.6 ​mm
Length: 7 ​mm
72 rats (Mg–Y-Nd-HRE 36 rats)
(Titanium 36 rats)
femur sections parallel to the long axis of the implants 24 weeks Differential blood count from blood sample obtained at sacrifice, IL-6 enzyme-linked immunosorbent assay, histology systemic inflammatory reactions (lobulated neutrophil granulocytes, stab neutrophils, lymphocytes, eosinophil granulocytes or basophil granulocytes), IL-6 enzyme
Erdmann et al. [51] 2010 MgCa0.8 (Stainless steel 316L screws as control)
Shape: screws
Diameter: 4 ​mm
Length: 6.0 ​mm
Screw head: 8.0 ​mm
40 rabbits (MgCa0.8 24 rabbits)
(Stainless steel 16 rabbits)
tibia part of muscle adjacent to the screw head 8 weeks histology, immunohistochemical staining macrophages, giant cells, heterophil granulocytes, lymphocytes, B and T-lymphocytes
Bondarenko et al. [52] 2011 MgCa0.8 (Titanium, PLA group as control)
Shape: N/A
Diameter: 2.5 ​mm
Length: 25 ​mm
9 rabbits (MgCa0.8 5 rabbits)
(Titanium 2 rabbits)
(PLA 2 rabbits)
tibia popliteal lymph node 6 months lymph node histology and immunohistochemistry heterophiles, B-cells, T-cells, histiocytes
Dziuba et al. [53] 2012 ZEK100 (Sham group as a control)
Shape: cylindrical
Diameter: 2.5 ​mm
Length: 25 ​mm
10 rabbits (7 animals-implant in both legs)
(3 animals-one leg implant, other sham)
tibia bone specimen containing implant 12 months histology macrophages, foreign body giant cells
Willbold et al. [54] 2013 RS66 Mg alloy
Shape: cylindrical
Diameter: 3 ​mm
Height: 5 ​mm
30 rabbits femur bone sample 8 weeks histology macrophages, neutrophils
Reifenrath et al. [55] 2013 ZEK100 Mg alloy
Shape: screws
Head diameter: 8.0 ​mm
Length: 5.0 ​mm
6 rabbits tibia muscle part directly adjacent to the screw head 6 weeks Immunohistochemical staining fibrous encapsulation, macrophages, giant cells and heterophil granulocytes, B- and T- lymphocytes
Waizy et al. [56] 2014 MgYREZr
Shape: screws
Shaft diameter: 2.0 ​mm
Bore diameter: 1.3 ​mm
Length: 20 ​mm
15 rabbits femur sections of bone perpendicular to the implant 12 months histology fibrous encapsulation
Pichler et al. [19] 2014 ZX50
WZ21
Shape: cylindrical pins
Diameter: 1.6 ​mm
Length: 8 ​mm
18 rats (6 rats sham group)
(6 rats ZX50)
(6 rats WZ21)
femur ND 24 weeks phagocytic assay, flow cytometry analysis neutrophil granulocytes
Willbold et al. [57] 2015 Mg–Ce, Mg–La, Mg–Nd
Shape: cylinders
Diameter: 2.99 ​± ​0.01 ​mm
Length: 5.00 ​± ​0.02 ​mm
9 rabbits (3 rabbits Mg–Ce)
(3 rabbits Mg–La)
(3 rabbits Mg–Nd)
femur bone sample 4 weeks histology foreign body reaction, encapsulation
Rossig et al. [58] 2015 LAE442 magnesium-based alloy (stainless austenitic steel as a control)
Shape: nails/screws,
Diameter: 9 mm/3.5 ​mm
Length: 130 mm/15–40 ​mm
10 sheep tibia bone sample 24 weeks histology, blood sample lymphocytes, macrophages, fibroblasts
Tie et al. [59] 2016 Mg–1Sr alloy,
Pure Mg, (sham as a control)
Shape: plates/screws
18 rabbits (6 ​Mg–1Sr alloy)
(6 pure Mg)
(6 sham)
femur muscle perpendicular to the implantation site, spleen, kidney, liver 16 weeks histopathology, haematology T-cells, red blood cells, white blood cells, albumin, LDH, liver enzymes, bilirubin
Diekmann et al. [60] 2016 MgYREZr (Ti6Al4v as a control)
Shape: screws
Diameter: 2.6 ​mm
Length: 10 ​mm
Thread pitch: 0.8 ​mm
36 rabbits (18 rabbits MgYREZr)
(18 rabbits
Ti6Al4v control)
tibia bone sample 24 weeks histology macrophages, granulocytes
Angrisani et al. [61] 2016 LAE442 magnesium-based alloy
Shape: cylinders
Diameter: 2.5 ​mm
Length: 25 ​mm
8 rabbits tibia bone sample 9 months to 3.5 years Histology, autopsy giant cells, macrophages, eosinophilic infiltrates, eosinophilic granulocytes
Wang et al. [62] 2017 High purity Mg (Ti screws as a control)
Shape: screws
Diameter: 3 ​mm
Length: 8 ​mm
64 rabbits tibia and femur bone sample 16 weeks histology macrophages, TGF beta 1
Kim et al. [63] 2018 Mg–Ca–Zn alloy (Polymeric mixture as a control)
Shape: plates and screws
Length, width, thickness: 24.5 ​mm ​× ​5.00 ​mm x 1.35 ​mm
6 male beagles zygomatic bone bone-implant interspace 4 weeks Biochemistry, complete blood count, blood coagulation panels, histology white blood count, macrophages, polymorphonuclear cells, lymphocytes, plasma cells, giant cells
Rahmati et al. [64] 2021 Mg–Ca–Zn (ZX00) alloy
(Sham as a control)
Shape: pins
Diameter: 1.6 ​mm
Length: 8 ​mm
12 rats femur bone sample 10 days Enzyme histochemical analysis, immunohistochemistry Osteoblast and osteoclast balance, M1 and M2 macrophages

ND; not done, N/A; not available.