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. 2022 Jun 22;57(25):12161–12175. doi: 10.1007/s10853-022-07349-8

Table 1.

Representative examples of polySP electrochemical synthesis

Electrochemical technique Experimental conditions Monomer concentration Working solution References
CV Applied potential: 0.2–0.7 V; scan-rate: 50 mVs−1; no. of cycles: 3 2 mM 50 mM NaCl solution in water [10]
CV Applied potential: 0–1 V; scan-rate: 150 mVs−1; no. of cycles: 5–20 0.5 mM 100 mM NaCl solution in water [20]
CV Applied potential: 0–1 V; scan-rate: 150 mVs−1; no. of cycles: 3 1 mM Phosphate buffer solution (PBS) [22]
CV Applied potential: 0–1 V; scan-rate: 20 mVs−1; no. of cycles: 3 1 mM 100 mM NaCl solution in water [21]
AT Applied pulsed potential: 0 V for 15 s; 0.5 V for 35 s vs Ag/AgCl; Pulse pairs: 30 0.5 mM Phosphate buffer solution (PBS) [31]
AT Applied pulsed potential: 0 V for 5 s; 0.7 V for 1 s; Pulse pairs: 30 0.5 mM 10 mM NaCl and 5% v/v ethanol in water [32]
AT Applied pulsed potential: 0 V for 5 s; 0.9 V for 1 s; Pulse pairs: 30 0.5 mM 10 mM NaCl solution in water [33]
AT Applied pulsed potential: 0 V for 5 s; 0.9 V for 1 s; Pulse pairs: 50 0.5 mM 100 mM NaCl solution in water [18]