Table 1.
Representative examples of polySP electrochemical synthesis
| Electrochemical technique | Experimental conditions | Monomer concentration | Working solution | References |
|---|---|---|---|---|
| CV | Applied potential: 0.2–0.7 V; scan-rate: 50 mVs−1; no. of cycles: 3 | 2 mM | 50 mM NaCl solution in water | [10] |
| CV | Applied potential: 0–1 V; scan-rate: 150 mVs−1; no. of cycles: 5–20 | 0.5 mM | 100 mM NaCl solution in water | [20] |
| CV | Applied potential: 0–1 V; scan-rate: 150 mVs−1; no. of cycles: 3 | 1 mM | Phosphate buffer solution (PBS) | [22] |
| CV | Applied potential: 0–1 V; scan-rate: 20 mVs−1; no. of cycles: 3 | 1 mM | 100 mM NaCl solution in water | [21] |
| AT | Applied pulsed potential: 0 V for 15 s; 0.5 V for 35 s vs Ag/AgCl; Pulse pairs: 30 | 0.5 mM | Phosphate buffer solution (PBS) | [31] |
| AT | Applied pulsed potential: 0 V for 5 s; 0.7 V for 1 s; Pulse pairs: 30 | 0.5 mM | 10 mM NaCl and 5% v/v ethanol in water | [32] |
| AT | Applied pulsed potential: 0 V for 5 s; 0.9 V for 1 s; Pulse pairs: 30 | 0.5 mM | 10 mM NaCl solution in water | [33] |
| AT | Applied pulsed potential: 0 V for 5 s; 0.9 V for 1 s; Pulse pairs: 50 | 0.5 mM | 100 mM NaCl solution in water | [18] |