TABLE 4.
Recovery of tetramethylpyrazine, ferulic acid, nodakenin, isoimperatorin in Chuanxiong Chatiao powder.
| Component | Content in the sample (ng/ml) | Amount of control product added (ng/ml) | Measured value (ng/ml) | Recovery rate (%) | RSD (%) |
|---|---|---|---|---|---|
| Tetramethylpyrazine | 7.44 | 3.70 | 11.16 | 100.54 | 1.07 |
| 7.69 | 3.70 | 11.42 | 100.81 | ||
| 7.31 | 3.70 | 11.00 | 99.73 | ||
| 7.38 | 7.40 | 14.58 | 97.30 | ||
| 7.52 | 7.40 | 14.87 | 99.32 | ||
| 7.64 | 7.40 | 14.95 | 98.78 | ||
| 7.43 | 11.10 | 18.36 | 98.47 | ||
| 7.47 | 11.10 | 18.47 | 99.10 | ||
| 7.35 | 11.10 | 18.40 | 99.55 | ||
| Ferulic acid | 831.81 | 420.51 | 1,251.03 | 99.69 | 1.75 |
| 843.74 | 420.51 | 1,260.30 | 99.06 | ||
| 840.97 | 420.51 | 1,250.71 | 97.44 | ||
| 855.39 | 841.02 | 1,725.30 | 103.44 | ||
| 850.65 | 841.02 | 1,706.12 | 101.72 | ||
| 861.93 | 841.02 | 1,701.77 | 98.86 | ||
| 847.20 | 1,261.53 | 2,100.04 | 99.31 | ||
| 856.55 | 1,261.53 | 2,108.56 | 99.25 | ||
| 860.12 | 1,261.53 | 2,117.93 | 99.71 | ||
| Nodakenin | 3,197.99 | 1,623.85 | 4,824.38 | 100.16 | 0.67 |
| 3,207.41 | 1,623.85 | 4,832.48 | 100.07 | ||
| 3,194.63 | 1,623.85 | 4,821.52 | 100.19 | ||
| 3,216.41 | 3,247.70 | 6,524.01 | 101.86 | ||
| 3,213.75 | 3,247.70 | 6,450.85 | 99.67 | ||
| 3,220.24 | 3,247.70 | 6,498.51 | 100.94 | ||
| 3,200.33 | 4,871.55 | 8,130.23 | 101.20 | ||
| 3,245.17 | 4,871.55 | 8,126.18 | 100.20 | ||
| 3,228.74 | 4,871.55 | 8,123.80 | 100.48 | ||
| Isoimperatorin | 14.31 | 7.25 | 21.74 | 102.48 | 1.84 |
| 14.57 | 7.25 | 21.68 | 98.07 | ||
| 14.43 | 7.25 | 21.78 | 103.17 | ||
| 14.55 | 14.50 | 29.41 | 102.48 | ||
| 14.60 | 14.50 | 29.14 | 100.28 | ||
| 14.68 | 14.50 | 29.47 | 102.00 | ||
| 14.54 | 21.75 | 36.03 | 98.80 | ||
| 14.65 | 21.75 | 36.29 | 99.49 | ||
| 14.48 | 21.75 | 36.16 | 99.68 |