Reaction conditions, yield, and purity of the synthesized compoundsa.
![]() | |||||||||
---|---|---|---|---|---|---|---|---|---|
Compound | Base | Time (h) | Yield (%) | Purity (%) | Compound | Base | Time (h) | Yield (%) | Purity (%) |
34 | 64 | 2 | 68 | 99.9 | 49 | 64 | 4 | 77 | 98.6 |
35 | 64 | 2 | 52 | 95.9 | 50 | 64 | 4 | 30 | N.D. |
36 | 64 | 2 | 96 | 99.3 | 51 | 64 | 4 | 26 | 98.7 |
37 | 64 | 2 | 58 | 99.0 | 52 | 64 | 4 | 44 | 99.3 |
38 | 64 | 2 | 87 | 99.7 | 53 | 64 | 4 | 53 | 98.0 |
39 | 64 | 3 | 75 | 99.7 | 54 | 64 | 4 | 58 | 96.2 |
40 | 64 | 3 | 62 | 98.9 | 55 | 64 | 4 | 40 | 99.1 |
41 | 64 | 3 | 65 | 97.3 | 56 | 64 | 4 | 11 | 97.1 |
42 | 64 | 3 | 50 | 98.7 | 57 | 64 | 5 | 56 | 95.1 |
43 | 64 | 3 | 82 | 96.0 | 58 | 64 | 5 | 92 | 99.1 |
44 | 64 | 3 | 16 | 99.4 | 59 | 65 | 3 | 27 | 96.6 |
45 | 64 | 3 | 56 | 98.8 | 60 | 65 | 3 | 69 | 98.7 |
46 | 64 | 3 | 58 | 97.9 | 61 | 65 | 3 | 59 | 97.9 |
47 | 64 | 3 | 48 | 97.9 | 62 | 66 | 4 | 24 | 97.1 |
48 | 64 | 3 | 76 | 99.6 | 63 | 66 | 3 | 56 | 98.3 |
N.D. = not determined.