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. 2022 Jun 23;12(29):18507–18523. doi: 10.1039/d2ra01814d

Reaction conditions, yield, and purity of the synthesized compoundsa.

graphic file with name d2ra01814d-u1.jpg
Compound Base Time (h) Yield (%) Purity (%) Compound Base Time (h) Yield (%) Purity (%)
34 64 2 68 99.9 49 64 4 77 98.6
35 64 2 52 95.9 50 64 4 30 N.D.
36 64 2 96 99.3 51 64 4 26 98.7
37 64 2 58 99.0 52 64 4 44 99.3
38 64 2 87 99.7 53 64 4 53 98.0
39 64 3 75 99.7 54 64 4 58 96.2
40 64 3 62 98.9 55 64 4 40 99.1
41 64 3 65 97.3 56 64 4 11 97.1
42 64 3 50 98.7 57 64 5 56 95.1
43 64 3 82 96.0 58 64 5 92 99.1
44 64 3 16 99.4 59 65 3 27 96.6
45 64 3 56 98.8 60 65 3 69 98.7
46 64 3 58 97.9 61 65 3 59 97.9
47 64 3 48 97.9 62 66 4 24 97.1
48 64 3 76 99.6 63 66 3 56 98.3
a

N.D. = not determined.