Table 1.
Crystal information of complexes 1 and 2
| Identification code | 1 | 2 |
|---|---|---|
| Empirical formula | C12H14MnN6O8 | C24H14MnN12O8 |
| Formula weight | 425.23 | 653.41 |
| Temperature/K | 296.15 | 296.15 |
| Crystal system | triclinic | triclinic |
| Space group | P-1 | P-1 |
| a/Å | 7.126(2) | 7.256(2) |
| b/Å | 7.8640(10) | 10.4125(14) |
| c/Å | 8.029(3) | 12.5589(12) |
| α/° | 65.136(4) | 73.8710(10) |
| β/° | 89.067(2) | 84.962(5) |
| γ/° | 70.0950(10) | 79.872(3) |
| Volume/Å3 | 379.57(18) | 896.6(3) |
| Z | 1 | 1 |
| ρcalcg/cm3 | 1.860 | 1.210 |
| μ/mm−1 | 0.934 | 0.424 |
| Data/restraints/parameters | 1390/0/124 | 3704/30/212 |
| Goodness-of-fit on F2 | 1.035 | 1.054 |
| Final R indexes [I ≥ 2σ (I)] | R1 = 0.0795, ωR2 = 0.2146 | R1 = 0.0433, ωR2 = 0.1132 |
| Final R indexes [all data] | R1 = 0.0918, ωR2 = 0.2283 | R1 = 0.0520, ωR2 = 0.1175 |
| Largest diff. peak/hole/e Å−3 | 0.88/-1.71 | 0.76/-0.82 |
| CCDC | 2119627 | 2,119,628 |