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. 2022 Jun 12;27(12):3781. doi: 10.3390/molecules27123781

Table 1.

Selected parameters for investigated compounds.

Compound The Dihedral Angle between Benzene Rings/° Aliphatic Chain Conformation OH‧‧‧OH Distance /Å Density/g cm−3 Melting Point/°C CSD Code
1,2-bis[2-(hydroxyformyl)phenoxy]methylene 59.43 gauche 9.815(2) 1.332 121–123 ref. [26] FASCUY [27]
1,2-bis[2-(hydroxyformyl)phenoxy]ethylene 60.89 trans–gauchetrans 6.446(4) 1.242 122–124 ref. [23] SAZCIF [28]
1,2-bis[2-(hydroxyformyl)phenoxy]propylene 80.73
84.59
transgauche-gauchetrans 9.659(2)
9.725(2)
1.274 96 ref. [23] FASDAF [27]
Do4OH 0 all-trans 13.754(2) 1.236 98 This work
Do5OH 84.2(1) transgauchetransgauchetrans 11.133(2) 1.268 64 This work
Do6OH I 0 all-trans 13.954(2)–conformer A
15.799(2)–conformer B
1.188 63 This work
Do6OH II 0 transgauchetranstranstransgauche-trans 13.461(2) 1.242 60 This work