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. 2022 Jun 3;20(6):377. doi: 10.3390/md20060377

Table 1.

1H/13C chemical shifts of dHfFS-1 obtained by peroxidative depolymerization from HfFS.

Residue Chemical Shift (ppm)
1 2 3 4 5 6
A
-l-Fuc2S4S-α(1,3)-
H 5.436 4.586 4.433 4.945 4.450 1.302
C 96.71 77.67 77.16 83.63 69.52 18.59
B
-l-Fuc-α(1,3)-
H 5.087 3.959 4.004 4.063 4.338 1.263
C 99.36 69.24 78.43 71.33 70.41 18.36
C
-l-Fuc-α(1,3)-
H 5.111 3.984 3.984 4.063 4.326 1.236
C 98.55 69.18 78.18 71.33 70.41 18.33
D
-l-Fuc2S-α(1,3)-
H 5.363 4.554 4.150 4.096 4.472 1.282
C 96.96 76.11 76.11 72.29 69.83 18.23
E
-l-Fuc2S-α(1,3)-
H 5.389 4.554 4.368 4.087 4.472 1.293
C 101.32 75.91 75.62 72.29 69.83 18.16