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94 GHz 19F Mims ENDOR spectra on F3Y122-β2/F2Y731-α2 (80 μM, TQ = 50 s, black lines) at T = 50 K. (A) Measurement with short τ values (∼250 ns). (B) Measurement with larger τ values (∼620 ns). Simulations including four different 19F atoms (Fa–Fd) are shown as blue lines and are based on S2 and S5 (Tables 1 and 2). Contributions of individual 19F atoms are shown as shaded areas: purple (Fa), cyan, (Fb), green (Fc), and brown (Fd).
