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. 2021 Sep 25;12(3):460–469. doi: 10.1016/j.jpha.2021.09.013

Table 1.

Chemical shift assignments in different fractions of GuiLingJi (GLJ).

No. Compounds Signals Fractions
1 Fatty acids or their ester or amides 0.880 (t, J = 7.2 Hz), 2.346 (t, J = 7.2 Hz), 2.015 (m), 2.771 (t, J = 6.6 Hz), 1.213–1.328, 5.348 (m) The chloroform fraction of GLJ (GLJ-C)
2 Triglycerides 4.146 (dd, J = 6, 12 Hz), 4.293 (dd, J = 4.2, 12 Hz) GLJ-C
3 β-rhamnosyl 1.146 (d, J = 6 Hz, CH3) The aqueous methanol fraction (GLJ-W/M)
4 Threonine 1.340 (d, J = 7.2 Hz) GLJ-W/M
5 Acetic acid 1.929 (s) GLJ-W/M
6 Succinate 2.432 (s) GLJ-W/M
7 Succinic acid 2.454 (s) GLJ-W/M
8 Creatine 3.059 (s), 3.960 (s) GLJ-W/M
9 Choline 3.216 (s) GLJ-W/M
10 Betaine 3.278 (s), 3.920 (s) GLJ-W/M
11 Glycine 3.689 (s) GLJ-W/M
12 Lactate 4.134 (q, J = 7.2 Hz) GLJ-W/M
13 Raffinose 4.964 (d, J = 4.2 Hz), 5.443 (d, J = 3.6 Hz) GLJ-W/M
14 Sucrose 5.422 (d, J = 4.2 Hz) GLJ-W/M
15 Formic acid 8.462 (s) GLJ-W/M