Table 2. Experimental details.
| Crystal data | |
| Chemical formula | KCoFe(PO4)2 |
| M r | 343.82 |
| Crystal system, space group | Monoclinic, C2/c |
| Temperature (K) | 296 |
| a, b, c (Å) | 13.5860 (6), 13.2320 (6), 8.7316 (4) |
| β (°) | 100.335 (2) |
| V (Å3) | 1544.21 (12) |
| Z | 8 |
| Radiation type | Mo Kα |
| μ (mm−1) | 4.99 |
| Crystal size (mm) | 0.36 × 0.27 × 0.15 |
| Data collection | |
| Diffractometer | Bruker D8 VENTURE Super DUO |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| T min, T max | 0.391, 0.747 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 30042, 3574, 2633 |
| R int | 0.068 |
| (sin θ/λ)max (Å−1) | 0.820 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.036, 0.088, 1.04 |
| No. of reflections | 3574 |
| No. of parameters | 118 |
| Δρmax, Δρmin (e Å−3) | 0.98, −0.91 |