Bruker APEXII CCD diffractometer | 6993 independent reflections |
Radiation source: micro-focus sealed tube | 6822 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.052 |
φ and ω scans | θmax = 30.5°, θmin = 2.1° |
Absorption correction: multi-scan (SADABS; Krause et al., 2015) | h = −15→15 |
Tmin = 0.520, Tmax = 0.746 | k = −14→14 |
58547 measured reflections | l = −16→16 |