Refinement on F2	Primary atom site location: structure-invariant direct methods
Least-squares matrix: full	Hydrogen site location: mixed
R[F2 > 2σ(F2)] = 0.067	H-atom parameters constrained
wR(F2) = 0.161	w = 1/[σ2(Fo2) + (0.0527P)2 + 4.2781P] where P = (Fo2 + 2Fc2)/3
S = 1.02	(Δ/σ)max < 0.001
9657 reflections	Δρmax = 0.67 e Å−3
629 parameters	Δρmin = −0.46 e Å−3
1 restraint