| Crystal data |
| Chemical formula |
[Ni(C10H24N4)(H2O)2]2[Ni(C10H24N4)(C27H24O9P3)2]·10H2O |
|
M
r
|
2200.09 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
160 |
|
a, b, c (Å) |
9.8779 (5), 17.2467 (11), 17.6707 (11) |
| α, β, γ (°) |
61.409 (6), 77.515 (5), 77.713 (5) |
|
V (Å3) |
2559.7 (3) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.72 |
| Crystal size (mm) |
0.40 × 0.10 × 0.10 |
| |
| Data collection |
| Diffractometer |
Rigaku Xcalibur Eos |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku OD, 2020 ▸) |
|
T
min, T
max
|
0.701, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
23737, 9657, 6598 |
|
R
int
|
0.063 |
| (sin θ/λ)max (Å−1) |
0.610 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.067, 0.161, 1.02 |
| No. of reflections |
9657 |
| No. of parameters |
629 |
| No. of restraints |
1 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.67, −0.46 |
