| Bruker D8 QUEST, Photon III detector diffractometer | 7370 independent reflections |
| Radiation source: fine-focus sealed X-Ray tube | 5962 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.057 |
| Detector resolution: 7.31 pixels mm-1 | θmax = 36.0°, θmin = 2.9° |
| φ and ω shutterless scans | h = −22→22 |
| Absorption correction: multi-scan (SADABS; Krause et al., 2015) | k = −22→22 |
| Tmin = 0.044, Tmax = 0.110 | l = −13→13 |
| 75835 measured reflections |