S1—N1 | 1.5139 (16) | C19—H19 | 0.9500 |
S1—N2 | 1.4838 (16) | C24—H24 | 1.0000 |
S1—O1 | 1.6257 (14) | C24—C25 | 1.537 (3) |
S1—C17 | 1.7718 (19) | C24—C26 | 1.539 (3) |
Si—N2 | 1.7240 (17) | C2—H2A | 0.9900 |
Si—C30 | 1.881 (2) | C2—H2B | 0.9900 |
Si—C24 | 1.882 (2) | C13—H13 | 0.9500 |
Si—C27 | 1.894 (2) | C13—C14 | 1.383 (3) |
O1—C1 | 1.452 (2) | C27—H27 | 1.0000 |
O2—C10 | 1.211 (2) | C27—C28 | 1.539 (3) |
O3—C3 | 1.211 (2) | C27—C29 | 1.539 (3) |
N1—C11 | 1.412 (2) | C8—H8 | 0.9500 |
N3—C3 | 1.396 (2) | C8—C7 | 1.394 (3) |
N3—C10 | 1.398 (2) | C28—H28A | 0.9800 |
N3—C2 | 1.459 (2) | C28—H28B | 0.9800 |
C17—C18 | 1.374 (3) | C28—H28C | 0.9800 |
C17—C22 | 1.392 (3) | C25—H25A | 0.9800 |
C11—C16 | 1.394 (3) | C25—H25B | 0.9800 |
C11—C12 | 1.394 (3) | C25—H25C | 0.9800 |
C4—C9 | 1.388 (3) | C5—H5 | 0.9500 |
C4—C3 | 1.489 (3) | C5—C6 | 1.392 (3) |
C4—C5 | 1.380 (3) | C15—H15 | 0.9500 |
C30—H30 | 1.0000 | C15—C14 | 1.386 (3) |
C30—C31 | 1.531 (3) | C14—H14 | 0.9500 |
C30—C32 | 1.525 (3) | C7—H7 | 0.9500 |
C16—H16 | 0.9500 | C7—C6 | 1.387 (3) |
C16—C15 | 1.389 (3) | C23—H23A | 0.9800 |
C9—C10 | 1.486 (3) | C23—H23B | 0.9800 |
C9—C8 | 1.385 (3) | C23—H23C | 0.9800 |
C20—C21 | 1.393 (3) | C26—H26A | 0.9800 |
C20—C19 | 1.392 (3) | C26—H26B | 0.9800 |
C20—C23 | 1.507 (3) | C26—H26C | 0.9800 |
C18—H18 | 0.9500 | C29—H29A | 0.9800 |
C18—C19 | 1.389 (3) | C29—H29B | 0.9800 |
C21—H21 | 0.9500 | C29—H29C | 0.9800 |
C21—C22 | 1.387 (3) | C6—H6 | 0.9500 |
C12—H12 | 0.9500 | C31—H31A | 0.9800 |
C12—C13 | 1.387 (3) | C31—H31B | 0.9800 |
C22—H22 | 0.9500 | C31—H31C | 0.9800 |
C1—H1A | 0.9900 | C32—H32A | 0.9800 |
C1—H1B | 0.9900 | C32—H32B | 0.9800 |
C1—C2 | 1.505 (3) | C32—H32C | 0.9800 |
O1—S1—C17 | 101.13 (8) | N3—C2—C1 | 113.82 (17) |
N1—S1—O1 | 105.93 (8) | N3—C2—H2A | 108.8 |
N1—S1—C17 | 101.98 (9) | N3—C2—H2B | 108.8 |
N2—S1—O1 | 107.27 (8) | C1—C2—H2A | 108.8 |
N2—S1—N1 | 126.60 (9) | C1—C2—H2B | 108.8 |
N2—S1—C17 | 111.06 (9) | H2A—C2—H2B | 107.7 |
N2—Si—C30 | 107.57 (9) | C12—C13—H13 | 119.6 |
N2—Si—C24 | 110.09 (9) | C14—C13—C12 | 120.8 (2) |
S1—N2—Si | 142.24 (11) | C14—C13—H13 | 119.6 |
N2—Si—C27 | 105.99 (9) | Si—C27—H27 | 106.6 |
C30—Si—C24 | 110.30 (9) | C28—C27—Si | 114.45 (15) |
C30—Si—C27 | 111.23 (9) | C28—C27—H27 | 106.6 |
C24—Si—C27 | 111.50 (9) | C29—C27—Si | 112.48 (14) |
C1—O1—S1 | 118.87 (12) | C29—C27—H27 | 106.6 |
C11—N1—S1 | 125.44 (14) | C29—C27—C28 | 109.50 (17) |
C3—N3—C10 | 112.05 (16) | C9—C8—H8 | 121.6 |
C3—N3—C2 | 123.98 (16) | C9—C8—C7 | 116.8 (2) |
C10—N3—C2 | 122.95 (16) | C7—C8—H8 | 121.6 |
C18—C17—S1 | 119.20 (15) | C27—C28—H28A | 109.5 |
C18—C17—C22 | 120.93 (18) | C27—C28—H28B | 109.5 |
C22—C17—S1 | 119.81 (15) | C27—C28—H28C | 109.5 |
C16—C11—N1 | 116.63 (18) | H28A—C28—H28B | 109.5 |
C12—C11—N1 | 124.22 (17) | H28A—C28—H28C | 109.5 |
C12—C11—C16 | 119.04 (19) | H28B—C28—H28C | 109.5 |
C9—C4—C3 | 108.23 (18) | C24—C25—H25A | 109.5 |
C5—C4—C9 | 121.8 (2) | C24—C25—H25B | 109.5 |
C5—C4—C3 | 129.93 (19) | C24—C25—H25C | 109.5 |
Si—C30—H30 | 107.8 | H25A—C25—H25B | 109.5 |
C31—C30—Si | 111.13 (14) | H25A—C25—H25C | 109.5 |
C31—C30—H30 | 107.8 | H25B—C25—H25C | 109.5 |
C32—C30—Si | 112.26 (14) | C4—C5—H5 | 121.5 |
C32—C30—H30 | 107.8 | C4—C5—C6 | 117.0 (2) |
C32—C30—C31 | 110.0 (2) | C6—C5—H5 | 121.5 |
C11—C16—H16 | 119.9 | C16—C15—H15 | 119.7 |
C15—C16—C11 | 120.2 (2) | C14—C15—C16 | 120.6 (2) |
C15—C16—H16 | 119.9 | C14—C15—H15 | 119.7 |
C4—C9—C10 | 108.12 (18) | C13—C14—C15 | 119.2 (2) |
C8—C9—C4 | 121.5 (2) | C13—C14—H14 | 120.4 |
C8—C9—C10 | 130.3 (2) | C15—C14—H14 | 120.4 |
C21—C20—C23 | 121.1 (2) | C8—C7—H7 | 119.2 |
C19—C20—C21 | 118.59 (18) | C6—C7—C8 | 121.6 (2) |
C19—C20—C23 | 120.3 (2) | C6—C7—H7 | 119.2 |
C17—C18—H18 | 120.2 | C20—C23—H23A | 109.5 |
C17—C18—C19 | 119.65 (19) | C20—C23—H23B | 109.5 |
C19—C18—H18 | 120.2 | C20—C23—H23C | 109.5 |
O3—C3—N3 | 125.02 (18) | H23A—C23—H23B | 109.5 |
O3—C3—C4 | 129.27 (19) | H23A—C23—H23C | 109.5 |
N3—C3—C4 | 105.70 (16) | H23B—C23—H23C | 109.5 |
C20—C21—H21 | 119.4 | C24—C26—H26A | 109.5 |
C22—C21—C20 | 121.12 (19) | C24—C26—H26B | 109.5 |
C22—C21—H21 | 119.4 | C24—C26—H26C | 109.5 |
O2—C10—N3 | 124.20 (19) | H26A—C26—H26B | 109.5 |
O2—C10—C9 | 129.97 (19) | H26A—C26—H26C | 109.5 |
N3—C10—C9 | 105.82 (17) | H26B—C26—H26C | 109.5 |
C11—C12—H12 | 119.9 | C27—C29—H29A | 109.5 |
C13—C12—C11 | 120.15 (19) | C27—C29—H29B | 109.5 |
C13—C12—H12 | 119.9 | C27—C29—H29C | 109.5 |
C17—C22—H22 | 120.5 | H29A—C29—H29B | 109.5 |
C21—C22—C17 | 118.94 (19) | H29A—C29—H29C | 109.5 |
C21—C22—H22 | 120.5 | H29B—C29—H29C | 109.5 |
O1—C1—H1A | 110.2 | C5—C6—H6 | 119.4 |
O1—C1—H1B | 110.2 | C7—C6—C5 | 121.2 (2) |
O1—C1—C2 | 107.48 (15) | C7—C6—H6 | 119.4 |
H1A—C1—H1B | 108.5 | C30—C31—H31A | 109.5 |
C2—C1—H1A | 110.2 | C30—C31—H31B | 109.5 |
C2—C1—H1B | 110.2 | C30—C31—H31C | 109.5 |
C20—C19—H19 | 119.6 | H31A—C31—H31B | 109.5 |
C18—C19—C20 | 120.8 (2) | H31A—C31—H31C | 109.5 |
C18—C19—H19 | 119.6 | H31B—C31—H31C | 109.5 |
Si—C24—H24 | 106.0 | C30—C32—H32A | 109.5 |
C25—C24—Si | 113.53 (14) | C30—C32—H32B | 109.5 |
C25—C24—H24 | 106.0 | C30—C32—H32C | 109.5 |
C25—C24—C26 | 110.03 (18) | H32A—C32—H32B | 109.5 |
C26—C24—Si | 114.45 (14) | H32A—C32—H32C | 109.5 |
C26—C24—H24 | 106.0 | H32B—C32—H32C | 109.5 |
S1—O1—C1—C2 | 154.80 (13) | C9—C4—C3—N3 | −1.7 (2) |
S1—N1—C11—C16 | 153.82 (16) | C9—C4—C5—C6 | −0.5 (3) |
S1—N1—C11—C12 | −30.1 (3) | C9—C8—C7—C6 | −0.7 (3) |
S1—C17—C18—C19 | −177.16 (14) | C20—C21—C22—C17 | −0.5 (3) |
S1—C17—C22—C21 | 177.63 (15) | C18—C17—C22—C21 | 0.5 (3) |
O1—S1—N1—C11 | 71.56 (18) | C3—N3—C10—O2 | 176.21 (19) |
O1—S1—N2—Si | −143.37 (17) | C3—N3—C10—C9 | −2.9 (2) |
O1—S1—C17—C18 | −138.15 (15) | C3—N3—C2—C1 | 105.9 (2) |
O1—S1—C17—C22 | 44.69 (16) | C3—C4—C9—C10 | 0.0 (2) |
O1—C1—C2—N3 | −74.8 (2) | C3—C4—C9—C8 | −177.80 (19) |
N1—S1—O1—C1 | 176.34 (13) | C3—C4—C5—C6 | 177.5 (2) |
N1—S1—N2—Si | −17.3 (2) | C21—C20—C19—C18 | 0.4 (3) |
N1—S1—C17—C18 | 112.72 (16) | C10—N3—C3—O3 | −176.40 (19) |
N1—S1—C17—C22 | −64.45 (17) | C10—N3—C3—C4 | 2.9 (2) |
N1—C11—C16—C15 | 174.52 (18) | C10—N3—C2—C1 | −86.5 (2) |
N1—C11—C12—C13 | −174.88 (18) | C10—C9—C8—C7 | −177.2 (2) |
N2—S1—O1—C1 | −46.09 (15) | C12—C11—C16—C15 | −1.8 (3) |
N2—S1—N1—C11 | −55.1 (2) | C12—C13—C14—C15 | −1.8 (3) |
N2—S1—C17—C18 | −24.57 (18) | C22—C17—C18—C19 | 0.0 (3) |
N2—S1—C17—C22 | 158.26 (15) | C19—C20—C21—C22 | 0.1 (3) |
N2—Si—C30—C31 | 55.01 (18) | C24—Si—N2—S1 | −0.8 (2) |
N2—Si—C30—C32 | −68.60 (19) | C24—Si—C30—C31 | 175.10 (16) |
N2—Si—C24—C25 | −61.52 (17) | C24—Si—C30—C32 | 51.5 (2) |
N2—Si—C24—C26 | 171.01 (15) | C24—Si—C27—C28 | −157.85 (14) |
N2—Si—C27—C28 | −38.05 (17) | C24—Si—C27—C29 | 76.34 (17) |
N2—Si—C27—C29 | −163.87 (15) | C2—N3—C3—O3 | −7.7 (3) |
C17—S1—O1—C1 | 70.31 (14) | C2—N3—C3—C4 | 171.58 (17) |
C17—S1—N1—C11 | 176.97 (17) | C2—N3—C10—O2 | 7.4 (3) |
C17—S1—N2—Si | 106.97 (18) | C2—N3—C10—C9 | −171.74 (17) |
C17—C18—C19—C20 | −0.5 (3) | C27—Si—N2—S1 | −121.54 (18) |
C11—C16—C15—C14 | 0.6 (3) | C27—Si—C30—C31 | −60.64 (18) |
C11—C12—C13—C14 | 0.7 (3) | C27—Si—C30—C32 | 175.74 (17) |
C4—C9—C10—O2 | −177.3 (2) | C27—Si—C24—C25 | 55.82 (18) |
C4—C9—C10—N3 | 1.7 (2) | C27—Si—C24—C26 | −71.65 (18) |
C4—C9—C8—C7 | 0.0 (3) | C8—C9—C10—O2 | 0.2 (4) |
C4—C5—C6—C7 | −0.1 (3) | C8—C9—C10—N3 | 179.2 (2) |
C30—Si—N2—S1 | 119.40 (18) | C8—C7—C6—C5 | 0.7 (3) |
C30—Si—C24—C25 | 179.92 (15) | C5—C4—C9—C10 | 178.36 (18) |
C30—Si—C24—C26 | 52.46 (18) | C5—C4—C9—C8 | 0.6 (3) |
C30—Si—C27—C28 | 78.57 (17) | C5—C4—C3—O3 | −0.7 (4) |
C30—Si—C27—C29 | −47.24 (18) | C5—C4—C3—N3 | −179.9 (2) |
C16—C11—C12—C13 | 1.1 (3) | C23—C20—C21—C22 | 179.82 (19) |
C16—C15—C14—C13 | 1.2 (3) | C23—C20—C19—C18 | −179.31 (18) |
C9—C4—C3—O3 | 177.6 (2) |