| Crystal data |
| Chemical formula |
C32H41N3O3SSi |
|
M
r
|
575.83 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
8.6752 (2), 8.8765 (2), 20.2299 (6) |
| α, β, γ (°) |
78.107 (2), 87.922 (2), 89.512 (2) |
|
V (Å3) |
1523.37 (7) |
|
Z
|
2 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
1.61 |
| Crystal size (mm) |
0.21 × 0.16 × 0.06 |
| |
| Data collection |
| Diffractometer |
XtaLAB Synergy R, HyPix-Arc 150 |
| Absorption correction |
Gaussian (CrysAlis PRO; Rigaku, 2021 ▸) |
|
T
min, T
max
|
0.555, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
28106, 5410, 4426 |
|
R
int
|
0.047 |
| (sin θ/λ)max (Å−1) |
0.597 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.041, 0.108, 1.05 |
| No. of reflections |
5410 |
| No. of parameters |
368 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.56, −0.38 |
