C1—C6 | 1.388 (4) | C17—C18 | 1.512 (5) |
C1—C2 | 1.392 (4) | C17—H17A | 0.97 |
C1—N1 | 1.408 (3) | C17—H17B | 0.97 |
C2—C3 | 1.384 (5) | C18—N4 | 1.485 (6) |
C2—H2 | 0.93 | C18—H18A | 0.97 |
C3—C4 | 1.359 (6) | C18—H18B | 0.97 |
C3—H3 | 0.93 | C19—N4 | 1.465 (5) |
C4—C5 | 1.357 (5) | C19—C20 | 1.495 (4) |
C4—H4 | 0.93 | C19—H19A | 0.97 |
C5—C6 | 1.375 (5) | C19—H19B | 0.97 |
C5—H5 | 0.93 | C20—N3 | 1.451 (4) |
C6—H6 | 0.93 | C20—H20A | 0.97 |
C7—N1 | 1.445 (4) | C20—H20B | 0.97 |
C7—C8 | 1.494 (5) | C21—O1 | 1.197 (4) |
C7—H7A | 0.97 | C21—O2 | 1.211 (4) |
C7—H7B | 0.97 | C21—C22' | 1.502 (7) |
C8—N2 | 1.489 (5) | C21—C22 | 1.502 (7) |
C8—H8A | 0.97 | C22—F3 | 1.321 (6) |
C8—H8B | 0.97 | C22—F1 | 1.337 (7) |
C9—N2 | 1.464 (5) | C22—F2 | 1.343 (7) |
C9—C10 | 1.488 (5) | C22'—F2' | 1.06 (2) |
C9—H9A | 0.97 | C22'—F3' | 1.306 (19) |
C9—H9B | 0.97 | C22'—F1' | 1.346 (19) |
C10—N1 | 1.466 (4) | C23—O3 | 1.224 (5) |
C10—H10A | 0.97 | C23—O4 | 1.228 (5) |
C10—H10B | 0.97 | C23—C24' | 1.506 (6) |
C11—C16 | 1.386 (4) | C23—C24 | 1.506 (6) |
C11—C12 | 1.390 (4) | C24—F5 | 1.238 (5) |
C11—N3 | 1.417 (3) | C24—F6 | 1.319 (7) |
C12—C13 | 1.379 (4) | C24—F4 | 1.342 (7) |
C12—H12 | 0.93 | C24'—F5' | 1.151 (17) |
C13—C14 | 1.369 (5) | C24'—F4' | 1.32 (2) |
C13—H13 | 0.93 | C24'—F6' | 1.459 (17) |
C14—C15 | 1.368 (5) | N2—H21 | 0.8818 |
C14—H14 | 0.93 | N2—H22 | 0.8672 |
C15—C16 | 1.377 (5) | N4—H41 | 0.8621 |
C15—H15 | 0.93 | N4—H42 | 0.8861 |
C16—H16 | 0.93 | OW1—HW1A | 0.8501 |
C17—N3 | 1.471 (4) | OW1—HW1B | 0.8501 |
C6—C1—C2 | 116.9 (3) | N4—C18—H18B | 109.8 |
C6—C1—N1 | 122.0 (3) | C17—C18—H18B | 109.8 |
C2—C1—N1 | 121.1 (3) | H18A—C18—H18B | 108.2 |
C3—C2—C1 | 120.8 (3) | N4—C19—C20 | 110.7 (3) |
C3—C2—H2 | 119.6 | N4—C19—H19A | 109.5 |
C1—C2—H2 | 119.6 | C20—C19—H19A | 109.5 |
C4—C3—C2 | 120.8 (3) | N4—C19—H19B | 109.5 |
C4—C3—H3 | 119.6 | C20—C19—H19B | 109.5 |
C2—C3—H3 | 119.6 | H19A—C19—H19B | 108.1 |
C5—C4—C3 | 119.2 (4) | N3—C20—C19 | 112.8 (3) |
C5—C4—H4 | 120.4 | N3—C20—H20A | 109 |
C3—C4—H4 | 120.4 | C19—C20—H20A | 109 |
C4—C5—C6 | 121.0 (4) | N3—C20—H20B | 109 |
C4—C5—H5 | 119.5 | C19—C20—H20B | 109 |
C6—C5—H5 | 119.5 | H20A—C20—H20B | 107.8 |
C5—C6—C1 | 121.2 (3) | O1—C21—O2 | 127.2 (4) |
C5—C6—H6 | 119.4 | O1—C21—C22' | 115.1 (4) |
C1—C6—H6 | 119.4 | O2—C21—C22' | 117.7 (4) |
N1—C7—C8 | 112.5 (3) | O1—C21—C22 | 115.1 (4) |
N1—C7—H7A | 109.1 | O2—C21—C22 | 117.7 (4) |
C8—C7—H7A | 109.1 | F3—C22—F1 | 103.5 (5) |
N1—C7—H7B | 109.1 | F3—C22—F2 | 108.8 (6) |
C8—C7—H7B | 109.1 | F1—C22—F2 | 100.9 (6) |
H7A—C7—H7B | 107.8 | F3—C22—C21 | 112.7 (4) |
N2—C8—C7 | 110.4 (3) | F1—C22—C21 | 112.9 (6) |
N2—C8—H8A | 109.6 | F2—C22—C21 | 116.7 (4) |
C7—C8—H8A | 109.6 | F2'—C22'—F3' | 112.1 (15) |
N2—C8—H8B | 109.6 | F2'—C22'—F1' | 110.0 (16) |
C7—C8—H8B | 109.6 | F3'—C22'—F1' | 103.4 (13) |
H8A—C8—H8B | 108.1 | F2'—C22'—C21 | 116.5 (11) |
N2—C9—C10 | 110.4 (3) | F3'—C22'—C21 | 106.9 (7) |
N2—C9—H9A | 109.6 | F1'—C22'—C21 | 107.0 (10) |
C10—C9—H9A | 109.6 | O3—C23—O4 | 127.7 (4) |
N2—C9—H9B | 109.6 | O3—C23—C24' | 115.5 (5) |
C10—C9—H9B | 109.6 | O4—C23—C24' | 116.8 (5) |
H9A—C9—H9B | 108.1 | O3—C23—C24 | 115.5 (5) |
N1—C10—C9 | 112.1 (3) | O4—C23—C24 | 116.8 (5) |
N1—C10—H10A | 109.2 | F5—C24—F6 | 111.9 (6) |
C9—C10—H10A | 109.2 | F5—C24—F4 | 104.5 (6) |
N1—C10—H10B | 109.2 | F6—C24—F4 | 96.7 (5) |
C9—C10—H10B | 109.2 | F5—C24—C23 | 115.4 (4) |
H10A—C10—H10B | 107.9 | F6—C24—C23 | 113.1 (4) |
C16—C11—C12 | 116.8 (3) | F4—C24—C23 | 113.6 (5) |
C16—C11—N3 | 121.0 (2) | F5'—C24'—F4' | 106.2 (16) |
C12—C11—N3 | 122.0 (3) | F5'—C24'—F6' | 103.6 (18) |
C13—C12—C11 | 121.1 (3) | F4'—C24'—F6' | 109.6 (11) |
C13—C12—H12 | 119.4 | F5'—C24'—C23 | 116.0 (8) |
C11—C12—H12 | 119.4 | F4'—C24'—C23 | 110.3 (9) |
C14—C13—C12 | 121.1 (3) | F6'—C24'—C23 | 110.7 (6) |
C14—C13—H13 | 119.4 | C1—N1—C7 | 116.1 (2) |
C12—C13—H13 | 119.4 | C1—N1—C10 | 115.0 (2) |
C15—C14—C13 | 118.3 (3) | C7—N1—C10 | 110.5 (2) |
C15—C14—H14 | 120.8 | C9—N2—C8 | 110.4 (3) |
C13—C14—H14 | 120.8 | C9—N2—H21 | 104.1 |
C14—C15—C16 | 121.2 (3) | C8—N2—H21 | 115 |
C14—C15—H15 | 119.4 | C9—N2—H22 | 115.8 |
C16—C15—H15 | 119.4 | C8—N2—H22 | 108.2 |
C15—C16—C11 | 121.4 (3) | H21—N2—H22 | 103.4 |
C15—C16—H16 | 119.3 | C11—N3—C20 | 115.9 (2) |
C11—C16—H16 | 119.3 | C11—N3—C17 | 114.7 (3) |
N3—C17—C18 | 111.9 (4) | C20—N3—C17 | 111.7 (2) |
N3—C17—H17A | 109.2 | C19—N4—C18 | 109.0 (3) |
C18—C17—H17A | 109.2 | C19—N4—H41 | 108.2 |
N3—C17—H17B | 109.2 | C18—N4—H41 | 116.5 |
C18—C17—H17B | 109.2 | C19—N4—H42 | 109.5 |
H17A—C17—H17B | 107.9 | C18—N4—H42 | 106.4 |
N4—C18—C17 | 109.5 (3) | H41—N4—H42 | 107.1 |
N4—C18—H18A | 109.8 | HW1A—OW1—HW1B | 104.5 |
C17—C18—H18A | 109.8 | ||
C6—C1—C2—C3 | 0.8 (4) | O3—C23—C24—F5 | −75.6 (8) |
N1—C1—C2—C3 | 179.7 (3) | O4—C23—C24—F5 | 103.6 (7) |
C1—C2—C3—C4 | −0.8 (5) | O3—C23—C24—F6 | 153.8 (6) |
C2—C3—C4—C5 | 0.1 (6) | O4—C23—C24—F6 | −26.9 (7) |
C3—C4—C5—C6 | 0.6 (6) | O3—C23—C24—F4 | 44.9 (7) |
C4—C5—C6—C1 | −0.5 (6) | O4—C23—C24—F4 | −135.8 (6) |
C2—C1—C6—C5 | −0.2 (5) | O3—C23—C24'—F5' | 102 (2) |
N1—C1—C6—C5 | −179.0 (3) | O4—C23—C24'—F5' | −79 (2) |
N1—C7—C8—N2 | 55.4 (4) | O3—C23—C24'—F4' | −18.9 (12) |
N2—C9—C10—N1 | −57.1 (5) | O4—C23—C24'—F4' | 160.3 (11) |
C16—C11—C12—C13 | −0.3 (5) | O3—C23—C24'—F6' | −140.4 (8) |
N3—C11—C12—C13 | 176.4 (3) | O4—C23—C24'—F6' | 38.8 (9) |
C11—C12—C13—C14 | 1.1 (5) | C6—C1—N1—C7 | −10.1 (4) |
C12—C13—C14—C15 | −1.1 (5) | C2—C1—N1—C7 | 171.1 (3) |
C13—C14—C15—C16 | 0.3 (5) | C6—C1—N1—C10 | −141.4 (3) |
C14—C15—C16—C11 | 0.5 (6) | C2—C1—N1—C10 | 39.8 (4) |
C12—C11—C16—C15 | −0.5 (5) | C8—C7—N1—C1 | 171.8 (3) |
N3—C11—C16—C15 | −177.2 (3) | C8—C7—N1—C10 | −54.8 (4) |
N3—C17—C18—N4 | 56.6 (5) | C9—C10—N1—C1 | −170.6 (3) |
N4—C19—C20—N3 | −55.9 (4) | C9—C10—N1—C7 | 55.5 (4) |
O1—C21—C22—F3 | −132.4 (6) | C10—C9—N2—C8 | 56.8 (4) |
O2—C21—C22—F3 | 49.2 (8) | C7—C8—N2—C9 | −55.8 (4) |
O1—C21—C22—F1 | 110.7 (6) | C16—C11—N3—C20 | −165.9 (3) |
O2—C21—C22—F1 | −67.7 (6) | C12—C11—N3—C20 | 17.6 (4) |
O1—C21—C22—F2 | −5.5 (8) | C16—C11—N3—C17 | −33.3 (4) |
O2—C21—C22—F2 | 176.1 (6) | C12—C11—N3—C17 | 150.2 (3) |
O1—C21—C22'—F2' | 47.1 (18) | C19—C20—N3—C11 | −174.6 (3) |
O2—C21—C22'—F2' | −131.3 (17) | C19—C20—N3—C17 | 51.5 (4) |
O1—C21—C22'—F3' | −79.2 (9) | C18—C17—N3—C11 | 173.3 (3) |
O2—C21—C22'—F3' | 102.4 (10) | C18—C17—N3—C20 | −52.1 (4) |
O1—C21—C22'—F1' | 170.6 (10) | C20—C19—N4—C18 | 59.6 (4) |
O2—C21—C22'—F1' | −7.8 (12) | C17—C18—N4—C19 | −60.0 (5) |