Refinement on F2 | Primary atom site location: structure-invariant direct methods |
Least-squares matrix: full | Secondary atom site location: structure-invariant direct methods |
R[F2 > 2σ(F2)] = 0.070 | Hydrogen site location: mixed |
wR(F2) = 0.235 | H-atom parameters constrained |
S = 1.07 | w = 1/[σ2(Fo2) + (0.1128P)2 + 0.3819P] where P = (Fo2 + 2Fc2)/3 |
4927 reflections | (Δ/σ)max < 0.001 |
375 parameters | Δρmax = 0.42 e Å−3 |
4 restraints | Δρmin = −0.28 e Å−3 |
0 constraints |