| Stoe IPDS 2T diffractometer | 1449 reflections with I > 2σ(I) |
| Radiation source: sealed X-ray tube, 12 x 0.4 mm long-fine focus | Rint = 0.046 |
| Plane graphite monochromator | θmax = 26.0°, θmin = 2.7° |
| Detector resolution: 6.67 pixels mm-1 | h = −10→9 |
| rotation method scans | k = −9→9 |
| 7437 measured reflections | l = −16→16 |
| 1762 independent reflections |
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