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. 2022 Jun 7;78(Pt 7):682–686. doi: 10.1107/S2056989022005643
Br1—C9 1.962 (2) Br1A—C9A 1.960 (3)
Br2—C10 1.965 (3) Br2A—C10A 1.979 (2)
O1—C7 1.362 (3) O1A—C7A 1.353 (3)
O1—C1 1.407 (3) O1A—C1A 1.403 (3)
O2—C7 1.196 (3) O2A—C7A 1.184 (3)
C1—C2 1.379 (3) C1A—C2A 1.379 (4)
C1—C6 1.383 (3) C1A—C6A 1.380 (3)
C2—C3 1.392 (3) C2A—C3A 1.390 (4)
C2—H2 0.9300 C2A—H2A 0.9300
C3—C4 1.392 (3) C3A—C4A 1.389 (3)
C3—C9 1.492 (3) C3A—C9A 1.498 (4)
C4—C5 1.389 (3) C4A—C5A 1.392 (3)
C4—H4 0.9300 C4A—H4A 0.9300
C5—C6 1.391 (3) C5A—C6A 1.391 (3)
C5—C10 1.495 (3) C5A—C10A 1.488 (3)
C6—H6 0.9300 C6A—H6A 0.9300
C7—C8 1.492 (3) C7A—C8A 1.494 (4)
C8—H8A 0.9600 C8A—H8A1 0.9600
C8—H8B 0.9600 C8A—H8A2 0.9600
C8—H8C 0.9600 C8A—H8A3 0.9600
C9—H9A 0.9700 C9A—H9A1 0.9700
C9—H9B 0.9700 C9A—H9A2 0.9700
C10—H10A 0.9700 C10A—H10C 0.9700
C10—H10B 0.9700 C10A—H10D 0.9700
C7—O1—C1 118.16 (18) C7A—O1A—C1A 118.43 (19)
C2—C1—C6 122.2 (2) C2A—C1A—C6A 121.8 (2)
C2—C1—O1 116.6 (2) C2A—C1A—O1A 119.6 (2)
C6—C1—O1 121.1 (2) C6A—C1A—O1A 118.3 (2)
C1—C2—C3 119.2 (2) C1A—C2A—C3A 119.3 (2)
C1—C2—H2 120.4 C1A—C2A—H2A 120.3
C3—C2—H2 120.4 C3A—C2A—H2A 120.3
C4—C3—C2 119.3 (2) C4A—C3A—C2A 119.4 (2)
C4—C3—C9 120.7 (2) C4A—C3A—C9A 120.0 (2)
C2—C3—C9 120.0 (2) C2A—C3A—C9A 120.5 (2)
C5—C4—C3 120.8 (2) C3A—C4A—C5A 121.0 (2)
C5—C4—H4 119.6 C3A—C4A—H4A 119.5
C3—C4—H4 119.6 C5A—C4A—H4A 119.5
C4—C5—C6 119.9 (2) C6A—C5A—C4A 119.2 (2)
C4—C5—C10 120.1 (2) C6A—C5A—C10A 120.1 (2)
C6—C5—C10 120.0 (2) C4A—C5A—C10A 120.7 (2)
C1—C6—C5 118.6 (2) C1A—C6A—C5A 119.3 (2)
C1—C6—H6 120.7 C1A—C6A—H6A 120.3
C5—C6—H6 120.7 C5A—C6A—H6A 120.3
O2—C7—O1 123.3 (2) O2A—C7A—O1A 122.4 (2)
O2—C7—C8 126.2 (2) O2A—C7A—C8A 126.0 (2)
O1—C7—C8 110.5 (2) O1A—C7A—C8A 111.6 (2)
C7—C8—H8A 109.5 C7A—C8A—H8A1 109.5
C7—C8—H8B 109.5 C7A—C8A—H8A2 109.5
H8A—C8—H8B 109.5 H8A1—C8A—H8A2 109.5
C7—C8—H8C 109.5 C7A—C8A—H8A3 109.5
H8A—C8—H8C 109.5 H8A1—C8A—H8A3 109.5
H8B—C8—H8C 109.5 H8A2—C8A—H8A3 109.5
C3—C9—Br1 111.76 (16) C3A—C9A—Br1A 112.24 (17)
C3—C9—H9A 109.3 C3A—C9A—H9A1 109.2
Br1—C9—H9A 109.3 Br1A—C9A—H9A1 109.2
C3—C9—H9B 109.3 C3A—C9A—H9A2 109.2
Br1—C9—H9B 109.3 Br1A—C9A—H9A2 109.2
H9A—C9—H9B 107.9 H9A1—C9A—H9A2 107.9
C5—C10—Br2 111.29 (17) C5A—C10A—Br2A 110.38 (16)
C5—C10—H10A 109.4 C5A—C10A—H10C 109.6
Br2—C10—H10A 109.4 Br2A—C10A—H10C 109.6
C5—C10—H10B 109.4 C5A—C10A—H10D 109.6
Br2—C10—H10B 109.4 Br2A—C10A—H10D 109.6
H10A—C10—H10B 108.0 H10C—C10A—H10D 108.1
C7—O1—C1—C2 −116.6 (2) C7A—O1A—C1A—C2A −81.9 (3)
C7—O1—C1—C6 66.7 (3) C7A—O1A—C1A—C6A 104.9 (3)
C6—C1—C2—C3 −0.8 (4) C6A—C1A—C2A—C3A 0.2 (3)
O1—C1—C2—C3 −177.5 (2) O1A—C1A—C2A—C3A −172.7 (2)
C1—C2—C3—C4 0.2 (3) C1A—C2A—C3A—C4A −0.4 (3)
C1—C2—C3—C9 −178.3 (2) C1A—C2A—C3A—C9A 175.3 (2)
C2—C3—C4—C5 0.4 (3) C2A—C3A—C4A—C5A 0.8 (3)
C9—C3—C4—C5 178.8 (2) C9A—C3A—C4A—C5A −175.0 (2)
C3—C4—C5—C6 −0.3 (3) C3A—C4A—C5A—C6A −0.9 (3)
C3—C4—C5—C10 177.8 (2) C3A—C4A—C5A—C10A 178.1 (2)
C2—C1—C6—C5 0.9 (4) C2A—C1A—C6A—C5A −0.3 (3)
O1—C1—C6—C5 177.4 (2) O1A—C1A—C6A—C5A 172.73 (19)
C4—C5—C6—C1 −0.3 (3) C4A—C5A—C6A—C1A 0.6 (3)
C10—C5—C6—C1 −178.5 (2) C10A—C5A—C6A—C1A −178.4 (2)
C1—O1—C7—O2 −4.0 (3) C1A—O1A—C7A—O2A −5.1 (4)
C1—O1—C7—C8 174.9 (2) C1A—O1A—C7A—C8A 175.6 (2)
C4—C3—C9—Br1 70.6 (2) C4A—C3A—C9A—Br1A −95.8 (3)
C2—C3—C9—Br1 −111.0 (2) C2A—C3A—C9A—Br1A 88.5 (3)
C4—C5—C10—Br2 80.7 (2) C6A—C5A—C10A—Br2A 99.1 (2)
C6—C5—C10—Br2 −101.1 (2) C4A—C5A—C10A—Br2A −79.9 (2)