| Bruker Kappa APEXII CCD area detector diffractometer | Rint = 0.058 |
| φ and ω scans | θmax = 29.4°, θmin = 2.7° |
| 11533 measured reflections | h = −5→4 |
| 1819 independent reflections | k = −16→16 |
| 1519 reflections with I > 2σ(I) | l = −20→20 |
| Bruker Kappa APEXII CCD area detector diffractometer | Rint = 0.058 |
| φ and ω scans | θmax = 29.4°, θmin = 2.7° |
| 11533 measured reflections | h = −5→4 |
| 1819 independent reflections | k = −16→16 |
| 1519 reflections with I > 2σ(I) | l = −20→20 |