Refinement on F2	Primary atom site location: structure-invariant direct methods
Least-squares matrix: full	Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.060	Hydrogen site location: mixed
wR(F2) = 0.109	H atoms treated by a mixture of independent and constrained refinement
S = 0.95	w = 1/[σ2(Fo2) + (0.0335P)2] where P = (Fo2 + 2Fc2)/3
4311 reflections	(Δ/σ)max < 0.001
399 parameters	Δρmax = 0.16 e Å−3
547 restraints	Δρmin = −0.16 e Å−3