| Crystal data |
| Chemical formula |
C22H19NO2
|
|
M
r
|
329.38 |
| Crystal system, space group |
Orthorhombic, P
b
c
n
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
20.8269 (2), 9.09843 (10), 9.0158 (1) |
|
V (Å3) |
1708.42 (3) |
|
Z
|
4 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
0.65 |
| Crystal size (mm) |
0.09 × 0.06 × 0.05 |
| |
| Data collection |
| Diffractometer |
XtaLAB Synergy, Dualflex, HyPix |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku OD, 2021 ▸) |
|
T
min, T
max
|
0.906, 0.939 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
21247, 1834, 1746 |
|
R
int
|
0.034 |
| (sin θ/λ)max (Å−1) |
0.637 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.051, 0.142, 1.09 |
| No. of reflections |
1834 |
| No. of parameters |
115 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.29, −0.23 |
