TABLE 3.
13C-NMR and 1H-NMR data of compounds 1 and 2.
| δC | δH mult (J) | |||
|  |  | |||
| No. | 1 | 2 | 1 | 2 | 
| 1 | 161.92 | 162.00 | ||
| 2 | 124.74 | 124.75 | 6.22 (d, 9.6 Hz, 1 H) | 6.25 (d, 9.7 Hz, 1 H) | 
| 3 | 141.26 | 140.52 | 7.16 (dd, 9.6, 5.9 Hz, 1 H) | 7.04 (dd, 9.7, 5.8 Hz, 1 H) | 
| 4 | 60.87 | 67.03 | 5.42 (dd, 6.0, 2.5 Hz, 1 H) | 5.45 (dd, 5.9, 2.7 Hz, 1 H) | 
| 5 | 79.27 | 80.43 | 4.45 (dd, 9.1, 2.5 Hz, 1 H) | 4.58 (dd, 6.8, 2.7 Hz, 1 H) | 
| 6 | 74.32 | 61.59 | 4.18 (m, 1 H) | 4.26 (q, 7.1 Hz, 1 H) | 
| 7 | 39.32 | 39.29 | 3.05 (dd, 16.9, 4.1 Hz, 1 H) 2.88 (dd, 16.9, 6.6 Hz, 1 H) | 2.81 (dd, 16.1, 3.8 Hz, 1 H) 2.75 (dd, 16.2, 7.4 Hz, 1 H) | 
| 8 | 210.41 | 211.00 | ||
| 9 | 73.16 | 73.68 | 4.37 (q, 7.2 Hz, 1 H) | 4.56–4.48 (m, 1 H) | 
| 10 | 19.35 | 19.18 | 1.43 (d, 7.12 Hz, 3 H) | 1.38 (d,7.1 Hz, 3 H) | 
| 11 | 59.04 | 3.32 (s, 1 H) | ||
| 1′ | 166.47 | 166.57 | ||
| 2′ | 127.54 | 127.36 | ||
| 3′ | 139.96 | 140.43 | 6.98–6.92 (m, 1 H) | 6.96–6.81 (m, 1 H) | 
| 4′ | 12.09 | 12.06 | 1.86–1.79 (m, 6 H) | 1.86–1.79 (m, 6 H) | 
| 5′ | 14.67 | 14.69 | ||
Bold values can make it easier for the reader to see the difference between the two compounds.