Table 4.
Sample | Freezing Time, Days |
Yield, % |
Cryogel Volume, cm3 |
Volume Shrinkage, % |
ρ, g/cm3 |
Porosity, % |
∆ V, % |
% |
SR, g/g |
E, kPa |
Crystallinity, % |
Specific Surface Area, m2/g |
---|---|---|---|---|---|---|---|---|---|---|---|---|
1 | 3 | 93.6 | 4.5 | 10.7 | 0.052 | 96.2 | 60 | 3319 | 8.7 | 1231 ± 132 | 28.2 | 38.062 |
7 | 10 | 90.0 | 1.43 | 71.4 | 0.157 | 88.6 | 66 | 3566 | 7.1 | 1099 ± 121 | 27.4 | 4.647 |
8 | 28 | 91.2 | 1.40 | 71.9 | 0.162 | 88.2 | 60 | 3336 | 5.1 | 2872 ± 478 | 26.8 | 16.765 |