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. 2022 Jun 24;22(13):4783. doi: 10.3390/s22134783

Table 2.

The facet area and area ratio of copper oxide polyhedral materials. Calculation based on the SEM images.

Sample Surface Composition Facet Area (µm)2 on Single Particle The Area Ratio of Facet on the Single Particle (%) The Intensity Ratio of Cu2O (111) and Cu2O (200) * γ(111)/(200)
(111) (110) (100) (011) (111) (110) (100) (011)
CC1 Cu2O/CuO 0.043 0.139 0.131 0.098 13.93 22.51 31.82 31.71 3.03
CC2 0.043 0.066 0.018 24.16 55.62 20.22 1.75
CC3 0.012 0.043 0.102 0.038 8.11 14.53 51.69 25.68 2.91
CC4 0.017 0.038 0.235 0.029 7.05 7.88 73.06 12.02 3.07
CC5 0.240 100 3.10

* The intensity ratios γ of copper oxide (200) and (111) planes may be evidence of the higher sensing/electrocatalytic activity due to the shifting toward lower potential values of initial glucose oxidation.