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Generation-collection experiments conducted at 2000 rpm in 0.1 M HClO4 on BDD and NDC–BDD (disk) and Pt NP-BDD (ring) RRDEs in oxygen-saturated and deaerated conditions: (a) LSVs on the NDC–BDD and BDD disk electrodes, scanned at 5 mV s–1. (b) Generated [H2O2] on the disk electrode vs disk potential for the oxygen-saturated solution.
