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. 2022 Jul 1;7(27):23576–23590. doi: 10.1021/acsomega.2c02151

Table 1. Textural and Quantitative Parameters of Mesoporous Samplesa.

   
 
pH-metric titration
N2 ad/desorption isotherms elemental analysis direct nack
sample SBET (m2/g) Vtotal (cm3/g) d (nm) N (%) C (%) H (%) CL (mmol/g) CL (mmol/g)
TEOS/EDTA 745 1.44 7.4         1.00  
NaSi/NH2 700 0.99 6.6 1.74 9.01 3.05 1.26 0.14 0.98
NaSi/EDTA/NH2 710 1.03 6.6 1.06 8.57 2.83 0.51/0.25 0.33/0.46 0.60/0.1
TEOS/QAS 730 1.12 7.0 0.92 9.53 3.1 0.82    
a

SBET – Surface area calculated by the BET method; Vtotal – volume of adsorbed N2 at p/po = 0.93; d – pore diameters calculated by BJH; CL −concentration of functional groups.