Table 1. Textural and Quantitative Parameters of Mesoporous Samplesa.
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pH-metric titration |
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| N2 ad/desorption isotherms | elemental analysis | direct | nack | ||||||
| sample | SBET (m2/g) | Vtotal (cm3/g) | d (nm) | N (%) | C (%) | H (%) | CL (mmol/g) | CL (mmol/g) | |
| TEOS/EDTA | 745 | 1.44 | 7.4 | 1.00 | |||||
| NaSi/NH2 | 700 | 0.99 | 6.6 | 1.74 | 9.01 | 3.05 | 1.26 | 0.14 | 0.98 |
| NaSi/EDTA/NH2 | 710 | 1.03 | 6.6 | 1.06 | 8.57 | 2.83 | 0.51/0.25 | 0.33/0.46 | 0.60/0.1 |
| TEOS/QAS | 730 | 1.12 | 7.0 | 0.92 | 9.53 | 3.1 | 0.82 | ||
SBET – Surface area calculated by the BET method; Vtotal – volume of adsorbed N2 at p/po = 0.93; d – pore diameters calculated by BJH; CL −concentration of functional groups.